NiMoO₄/g-C₃N₄ was fabricated by a hydrothermal method and used as an electrode material in a supercapacitor. The samples were characterized by XRD, FTIR, scanning electron microscopy (SEM) and transmission electron microscopy (TEM) to study the physical and structural properties of the as-prepared NiMoO₄/g-C₃N₄ material. The electrochemical responses of pristine NiMoO₄ and the NiMoO₄/g-C₃N₄ nanocomposite material were investigated by cyclic voltammetry (CV), galvanostatic charge-discharge (GCD) and electrochemical impedance spectroscopy (EIS). From the CD studies, the NiMoO₄/g-C₃N₄ nanocomposite revealed a higher maximum specific capacitance (510 Fg⁻¹) in comparison to pristine NiMoO₄ (203 Fg⁻¹). In addition, the NiMoO₄/g-C₃N₄ composite electrode material exhibited high stability, which maintained up to 91.8% capacity even after 2000 charge-discharge cycles. Finally, NiMoO₄/g-C₃N₄ was found to exhibit an energy density value of 11.3 Whkg⁻¹. These findings clearly suggested that NiMoO₄/g-C₃N₄ could be a suitable electrode material for electrochemical capacitors.

In the present study, the synthesis of CoWO₄ (CWO)–Ni nanocomposites was conducted using a wet chemical method. The crystalline phases and morphologies of the Ni nanoparticles, CWO, and CWO–Ni composites were analyzed using X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and energy-dispersive X-ray spectroscopy (EDAX). The electrochemical properties of CWO and CWO–Ni composite electrode materials were assessed by cyclic voltammetry (CV), and galvanostatic charge–discharge (GCD) tests using KOH as a supporting electrolyte. Among the CWO–Ni composites containing different amounts of Ni1, Ni2, and Ni3, CWO–Ni3 exhibited the highest specific capacitance of 271 F g⁻¹ at 1 A g⁻¹, which was greater than that of bare CWO (128 F g⁻¹). Moreover, the CWO–Ni3 composite electrode material displayed excellent reversible cyclic stability and maintained 86.4% of its initial capacitance after 1500 discharge cycles. The results obtained herein demonstrate that the prepared CWO–Ni3 nanocomposite is a promising electrode candidate for supercapacitor applications.

Bimetallic nanoparticles (NPs) exhibit advantageous electrical, optical, and catalytic properties. Among the various NP synthesis methods, pulsed laser ablation in liquid (PLAL) is currently attracting much attention because of its simplicity and versatility. In this study, a pulsed laser was used to produce nickel/palladium (Ni/Pd) bimetallic NPs in methanol and deionized water. The morphological and optical properties of the resulting Ni/Pd bimetallic NPs were characterized. The synthesized Ni/Pd bimetallic NPs were used for the dechlorination of 1,2-dichlorobenzene (1,2-DCB) under various conditions. The dechlorination rates of 1,2-DCB while using single (Ni and Pd) and bimetallic (Ni powder/Pd and Ni/Pd) NPs were investigated. The results showed that the Ni/Pd bimetallic NPs with 19.16 wt.% Pd exhibited much enhanced degradation efficiency for 1,2-DCB (100% degradation after 30 min). Accordingly, the results of enhanced the degradation of 1,2-DCB provide plausible mechanism insights into the catalytic reaction.