As electronic cigarettes (e-cigarettes) represent a new constantly evolving product category, the systematic analysis of the developed devices and the e-liquid vaporization is challenging. Indeed, understanding how e-cigarettes work and the role of key parameters in the process are major issues. This work focuses on an experimental study of how the power supplied by the battery to the atomizer coil influences e-liquid consumption. The reproducibility and the repeatability of e-liquid consumption were investigated over 20 series of 20 puffs for one of the tested atomizers. Then, the reproducibility and the repeatability of the e-liquid consumption was investigated over five series of 20 puffs for each tested atomizer. The wire behavior according to the supplied power could be separated into three regimes: under-heating (insufficient power to generate an aerosol), optimal vaporization characterized by a linear trend (vaporization of the e-liquid proportional to the supplied energy) and over-heating (dry-burn occurs). Using a controllable and repeatable energy supply, the reproducibility of the quantity of vaporized e-liquid was verified for each of the five series of 20 puffs programed for all the atomizers except one. Finally, the influence of the supplied power on the vaporization and the consumption of the e-liquid as well as the optimal power ranges were investigated and discussed. The results showed that atomizers with resistance ranging from 1 Ω to 1.8 Ω are efficient using all the energy supplied by the battery to vaporize the e-liquid and reducing the energy lost in the cotton or in the metal part of atomizer coil.
The accurate study of aerosol composition and nicotine release by electronic cigarettes is a major issue. In order to fully and correctly characterize aerosol, emission generation has to be completely mastered. This study describes an original vaping machine named Universal System for Analysis of Vaping (U-SAV), dedicated to vaping product study, enabling the control and real-time monitoring of applied flow rate and power. Repeatability and stability of the machine are demonstrated on flow rate, power regulation and e-liquid consumption. The emission protocol used to characterize the vaping machine is based on the AFNOR-XP-D90-300-3 standard (15 W power, 1 Ω atomizer resistance, 100 puffs collected per session, 1.1 L/min airflow rate). Each of the parameters has been verified with two standardized liquids by studying mass variations, power regulation and flow rate stability. U-SAV presents the required and necessary stability for the full control of emission generation. The U-SAV is recognised by the French association for standardization (AFNOR), European Committee for Standardization (CEN) and International Standards Organisation (ISO) as a vaping machine. It can be used to highlight the influence of the e-liquid composition, user behaviour and nature of the device, on the e-liquid consumption and aerosol composition.
This work focuses on an experimental study of the influence of e-liquid composition on the mass of vaporized e-liquid after standardized emission generation using a U-SAV (Universal System for Analysis of Vaping) vaping machine. All the experiments were based on the use of a Cubis 1Ω clearomiser and on the standard protocol for electronic cigarettes emission generation. Currently, there is no standardized method available to calibrate the emission generations of electronic cigarettes. Since the e-liquid compositions are not always known, we propose a simple, practical, effective, and fast method of emission generation calibration. Therefore, this paper examines a major issue in this new and constantly evolving field, allowing the validation of the emission generation results. To our knowledge, this method is a novelty in our discipline and could be easily developed in laboratories. Pure propylene-glycol, glycerol, ethanol, and water and their mixtures (20 e-liquids) were tested as reference materials, allowing an e-liquids benchmarking and the characterization of 800 commercial e-liquids (with known and unknown compositions) at a fixed power and for one inhalation profile (3 s puff duration and 55 mL of puff volume). The influence of ethanol and/or water addition in the e-liquid was characterized.