Based on the enhanced charge separation efficiency of the one-dimensional structure and strong surface plasmon resonance (SPR) of gold, a gold modified TiO₂ nanotube (Au/TiO₂NTs) glucose photoelectrochemical (PEC) sensor was prepared. It could be activated by visible red light (625 nm). Under optimal conditions, the Au/TiO₂NTs sensor exhibited a good sensitivity of 170.37 μA·mM⁻¹·cm⁻² in the range of 1–90 μM (R² = 0.9993), and a detection limit of 1.3 μM (S/N = 3). Due to its high selectivity, good anti-interference ability, and long-term stability, the fabricated Au/TiO₂NTs sensor provides practical detection of glucose. It is expected to be used in the construction of non-invasive PEC biosensors.

Gold catalysts have been studied in-depth due to their unique activities for catalytic CO oxidation. Supports have intrinsic motivation for the high activity of gold catalysts. Thermally stable urchin-like CuO microspheres, which are potential support for gold catalysts, were prepared by facile solution-method. Then gold nanoparticles were loaded on them by deposition-precipitation method. The obtained gold catalysts were characterized by SEM, XRD, TEM, BET, ICP, and XPS. Their catalytic activity for CO oxidation was also evaluated. TEM results revealed that the gold nanoparticles with small sizes were highly distributed on the CuO surface in Au_1.0/CuO-300. XPS observations demonstrated that the gold species in Au_1.0/CuO-300 was of metallic state. Among the as-prepared catalysts, the Au_1.0/CuO-300 catalyst displayed the best performance for CO oxidation and achieved 100% CO oxidation at 80 °C. It kept 100% conversion for 20 h at a reaction temperature of 180 °C, and showed good reusability after three reaction-cycles. The possible catalytic mechanism of Au_1.0/CuO-300 catalyst for CO oxidation was also briefly proposed.

Photocatalytic water splitting for hydrogen generation is a significant pathway for sustainable energy conversion and production. The photocatalysts with a Z-scheme water splitting charge transfer pathway is superior due to the good separation and migration ability of photoexcited charge carriers. Herein, Co₃O₄/g-C₃N₄ photocatalysts with Z-scheme charge transfer pathway were successfully constructed by an electrostatic interaction-annealing method. The as-prepared Co₃O₄/g-C₃N₄ ultra-thin nanosheets were tested and analyzed by XRD, EA, ICP, SEM, TEM, AFM, XPS, UV-Vis DRS, PL and photoelectrochemical measurements. Moreover, the influences of fabrication parameters on performance of Co₃O₄/g-C₃N₄ catalysts were investigated, and 0.5% Co₃O₄/g-C₃N₄ exhibited the optimal activity. Based on the characterization and catalytic performance, the Z-scheme charge transfer pathway of Co₃O₄/g-C₃N₄ was established and put forward. To further improve the catalytic performance of Co₃O₄/g-C₃N₄, 0.5% Pt was added as a co-catalyst. The obtained Pt/0.5% Co₃O₄/g-C₃N₄ was recyclable and remained the original catalytic water splitting performance within 20 h. The modification of Co₃O₄ and Pt improved the separation and migration of e⁻ and h⁺, and induced the increased hydrogen evolution rate of g-C₃N₄.