Nanoparticles with controllable sizes of ferrite spinel CoFe2O4 were formed by thermal treatment of cobalt-iron glycerolate. Thermal behavior during the heating was studied by differential thermal analysis combined with thermogravimetry. The precursor, as well as the prepared nanoparticles, were analyzed by a broad spectrum of analytic techniques (X-Ray photoelectron spectroscopy (XPS), X-Ray diffraction (XRD), Energy dispersive spectroscopy (EDS), Atomic absorption spectroscopy (AAS), Scanning electron microscopy (SEM), and Raman spectroscopy). The particle size of nanoparticles was obtained from Transmission electron microscopy and also calculated using Scherrer formula. A vibrating sample magnetometer (VSM) in a Physical Property Measurement System was used to analyze the magnetic properties of nanoparticles.
Hydrotalcites are layered double hydroxides displaying a variety of stoichiometry caused by the different arrangement of the stacking of the layers, ordering of the metal cations, as well as the arrangement of anions and water molecules, in the interlayer galleries. The compounds of the hydrotalcite group show a wide range of the possible applications due to their specific properties, such as their large surface area, ion exchange ability, the insolubility in water and most of the organic sorbents, and others. Affordability, wide possibilities of manufacturing, and presence of sufficient natural deposits make hydrotalcites potentially very useful for the construction industry, as either a building material itself or an additive in mortars, concrete or in polymers composites used in constructions. Similar possible application of such material is in leakage control in a radioactive waste repository. The effect of use of these materials for ion exchange, anti-corrosion protection, radioactive ions containment, and similar purposes in building materials is examined in this review.
Since the discovery of high-temperature superconductivity, significant progress in the fabrication of REBCO-based (Rare Earth Barium Copper mixed Oxides) thin-films superconductors has been achieved. In our review, we described the approaches and possibilities of the improvement of superconducting properties by the introduction of nanosized pinning centers. We focused on the synthesis and viability of the material for artificial pinning centers and methods used for the introduction of the pinning centers into superconducting REBCO-based thin-films. This article summarizes available materials and procedures regardless of the financial cost of the individual method. According to available literature, the most significant superconducting REBCO tapes can be obtained when a combination of 1D and 0D nanoparticles are used for nanoscale pinning.
Spherical amorphous nano and microparticles of elemental selenium have been prepared by simple reduction method. For surface stabilisation, sodium dodecyl sulphate (SDS), polysorbate 80 and tryptone have been used. ZetaSizer and transmission electron microscopy measurements were used for characterisation of the size and shape of prepared particles and X‐ray diffraction measurements to confirm their amorphous nature. The sizes of the nanoparticles stabilised by SDS can be controlled by varying of the surfactant concentration. Particles stabilised by tryptone have microdimensions and could be therefore applied where nanodimensions are not suitable.