Designing a new family of advanced high-strength steels (AHSSs) to develop automotive parts that cover early industry needs is the aim of many investigations. One of the candidates in the 3rd family of AHSS are the quenching and partitioning (QP) steels. These steels display an excellent relationship between strength and formability, making them able to fulfill the requirements of safety, while reducing automobile weight to enhance the performance during service. The main attribute of QP steels is the TRIP effect that retained austenite possesses, which allows a significant energy absorption during deformation. The present study is focused on evaluating some process parameters, especially the partitioning temperature, in the microstructures and mechanical properties attained during a QP process. An experimental steel (0.2C-3.5Mn-1.5Si (wt%)) was selected and heated according to the theoretical optimum quenching temperature. For this purpose, heat treatments in a quenching dilatometry and further microstructural and mechanical characterization were carried out by SEM, XRD, EBSD, and hardness and tensile tests, respectively. The samples showed a significant increment in the retained austenite at an increasing partitioning temperature, but with strong penalization on the final ductility due to the large amount of fresh martensite obtained as well.

The major goal of this work was to study the effect of rapid heating and fast cooling on the transformation behavior of 22MnB5 steel. The effect of the initial microstructure (ferrite + pearlite or fully spheroidized) on the transformation behavior of austenite (during intercritical and supercritical annealing) in terms of heating rates (2.5, 30 & 200 °C/s) and fast cooling, i.e., 300 °C/s rate, were studied. As expected, the kinetics of austenite nucleation and growth were strongly related to the heating rates. Similarly, the carbon content of the austenite was higher at lower intercritical annealing temperatures, particularly when slower heating rates were used. The supercritical temperatures used in this study were similar to those used during commercial hot stamping operations, i.e., 845 and 895 °C, respectively, followed by a fast cooling rate. The prior austenite grain size (PAGS) was not strongly influenced by the nature of the initial microstructure, heating rate, reheating temperatures (845 or 895 °C), at 30 s holding time. The decomposition of austenite using fast cooling rates was examined. The results showed that 100% martensite was not obtained. The observed low temperature transformation products consisted of mixtures of martensite-bainite plus undissolved Fe₃C carbides and small amounts of martensite-austenite (M-A). At higher supercritical temperatures, i.e., 1000 °C and 1050 °C, the final microstructure showed an increase in the volume fraction of martensite and a decrease in the volume fraction of bainite. The Fe₃C and the M-A microconstituent were not observed. The best combination of tensile properties was obtained on samples reheated in the lower temperature range (845 to 895 °C). Interestingly, when the samples where reheated at the higher temperature range (1000 to 1050 °C) and fast cooled, the results of the mechanical properties did not exhibit significantly higher strength levels independent of heating rate or initial microstructural condition. This can be attributed to the change in the microstructural balance %martensite+%bainite as the reheating temperature increases. The results of this study are presented and discussed.

The microstructure of a low Si, ultra-low-C, hot-rolled electrical steel strip is modified by annealing at T < To, the α→γ transformation temperature. This heat treatment causes the abnormal anisotropic growth of surface grains which consumes the original hot-rolled microstructure. The growth of the surface grains first takes place parallel to the rolling direction and then in a columnar form parallel to the normal direction until grains growing in opposite directions from the surfaces impinge at the center of the strip. It is shown that cold rolling and a short annealing treatment at temperatures between 700 and 800 °C leads to microstructures which result in iron energy losses that can be as much as 30% lower than those observed in the same material not subjected to the annealing prior to cold rolling. The magnitude of the reduction in energy losses depends on strip thickness and processing parameters. The major effect is observed in material annealed at 710 °C and the relative effect (with respect to material that is not annealed prior to cold rolling) decreases as the strip thickness decreases. It is shown that these effects can be attributed to the effect of the processing conditions on texture and grain size. The maximum reduction in energy losses is observed when the final microstructure consists of ferrite grains ~1.5 times larger than those obtained if the material is not annealed prior to cold rolling.

This study investigates the critical transformation temperatures of a high-strength API-grade steel through thermal analysis and software simulations; the precise determination of these temperatures is essential for enhancing the efficacy of subsequent experimental trials. Utilizing the ‘Quench Properties’ module of JMatPro^® V14, characteristic transformations were identified between 950 °C and 25 °C under stable conditions. Heating rates of 5, 10, and 30 °C/s were applied to determine critical temperatures, with Ac₁ ranging from 700 °C to 750 °C and Ac₃ from 850 °C to 900 °C. Niobium content may influence Ac₁ and Ac₃, promoting the ferritic phase and elevating transformation temperatures at a heating rate of 30 °C/s. Conversely, a rate of 10 °C/s significantly influenced austenite formation, impacting the development of microconstituents that enhance both strength and elongation post-quenching. Furthermore, slow cooling was found to favor the premature formation of allotriomorphic ferrite, which hinders the transformation of austenite into bainite and martensite during accelerated cooling. Finally, this study corroborates that JMatPro^® is a reliable tool for predicting critical temperatures and designing optimized thermomechanical processing routes.

The thermomechanical process to obtain high alloy high strength steels is based on the control of variables such as temperature, deformation and strain rate to promote hardening mechanisms that directly influence the strength and toughness of the steel. Experimentally, it was determined for an API type steel, that the temperature of potential precipitation during the hot deformation process will be in a range of temperature from 1150°C to 1000°C. Precipitation will occur instantaneously due to temperature, deformation and strain rate (0.1 and 0.2 deformation and 0.5s-1 and 1s-1 strain rate) effect. The incorporation of microalloying elements as Nb in a percentage of < 0.050 significantly influences precipitation hardening preferentially located at austenitic grain boundaries. It was determined that precipitates of between 3 to 5 nanometers in size, distinguished as NbC will be obtained. It was found that the precipitation kinetics for the steel is affected by a single step deformation applied, by the formation of precipitate colonies at 0.1 deformation and strain rate 1s-1, which does not allow the dispersion of precipitates generating a planar interface in the microstructure of the steel. Finally, the preferentially localized precipitation mechanism of the almost continuous type by the grain boundaries was evidenced. This mechanism is crucial for controlling austenitic grain size during deformation, which leads to a final, homogenized microstructure.

En este artículo se aborda la precipitación durante la laminación en caliente de aceros de alta resistencia, especialmente grados API. Se analizan el proceso termomecánico (T, Ԑ, ), el producto de solubilidad (Ks) y la cinética de precipitación inducida por deformación (Ps-Pf). El objetivo es proponer las condiciones termomecánicas y químicas dadas por la presencia de Nb, Ti y V que favorecen la precipitación de carburos de estos elementos en aceros HSLA (High Strength Low Alloy) buscando la modificación de la microestructura y las propiedades mecánicas.