Low permeability of wood causes problems during drying of timber. This study evaluated the effects of microwave (MW) pretreatment on the conventional drying behavior and mechanical damages of Chinese fir lumber. MW pretreatment of lumber was performed at applied MW energy of 43 kWh/m³, and then, the samples were dried in a laboratory drying kiln. The results showed that the drying rate was effectively increased after MW pretreatment. The moisture content (MC) deviation in thickness and residual stress indexes of MW-pretreated samples were significantly decreased in comparison with the control samples, and the appearance quality of wood samples was not clearly affected by the MW pretreatment. Scanning electron microscope (SEM) micrographs demonstrated that pit membranes were damaged after MW pretreatment, and the micro-cracks in radial section as well as detachments between ray parenchyma cells and tracheids were also observed. Consequently, new pathways for moisture migration during drying process were formed after MW pretreatment, which contributed to the improved permeability of Chinese fir lumber and decreased drying time.

Microwave (MW) treatment is an effective method to increase refractory wood permeability, thereby reducing drying time and defects. The extent of modification depends on the damage extent of the wood microstructure. In this study, MW intensities of 43 kWh/m³ (low intensity) and 57 kWh/m³(high intensity) were adopted to treat Chinese fir lumber. Microstructural changes in wood samples were observed using scanning electron microscopy (SEM) and pore structure was characterized using mercury intrusion porosimetry (MIP). Results were as follows: After low-intensity MW treatment, parts of the bordered pit membranes in tracheids were damaged, and micro-fibrils on the margo were ruptured, while the torus basically remained intact. Micro-cracks were observed at both ends of the cross-field pit apertures, propagating to the cell walls of tracheids. The middle lamellar between ray parenchyma cells and longitudinal tracheids cracked, and the width of cracks was in the range of 1–25 μm. After high-intensity MW treatment, damage to the wood microstructure was more severe than that in the low-intensity MW treatment, with macro-cracks having a width range of 100–130 μm being generated. In addition, on the fracture surface of macro-cracks, the bordered pit membranes in tracheids fell off, cross-field pit membranes disappeared and the ray parenchyma cells were seriously damaged, exhibiting fracture of the tracheid walls. Both low-intensity and high-intensity MW treatment can increase the pore diameter corresponding to the margo capillaries (peak value increased from 674.7 nm to 831.8 nm and 1047.6 nm, respectively). The number of pores in the tracheid lumen diameter range also significantly increased. These results provide a theoretical support forMW treatment processes’ improvement and high-value utilization of Chinese fir.

Due to wood moisture sensitivity, shrinkage cracks tend to present wooden structures. These failures are caused by moisture-related shrinkage behavior. In order to avoid it, it is necessary to have a better understanding of shrinkage behavior. In this respect, studying the dimension changes in wood at different scales is of utmost significance for a better understanding of the shrinkage properties. Herein, the shrinkage behavior of Masson pines (Pinus massoniana) wood was investigated at macroscopic and cellular levels during moisture loss via digital image correlation using VIC-3D and digital microscopic systems, respectively. According to the full-field strain maps, shrinkage strain near the external face was higher than that at the internal face, which increased susceptibility to cracking at the external face of lumber. Additionally, the anisotropic shrinkage of wood was explored. The shrinkage ratio at the end of drying was about 5.5% in the tangential (T) direction and 3.5% in the radial (R) direction. However, at a cellular level, the shrinkage ratios in the T and R directions of earlywood tracheids were 7.13% and 2.46%, whereas the corresponding values for latewood tracheid were 9.27% and 5.52%, respectively. Furthermore, the maximum T/R shrinkage ratio at the macroscopic level (1.7) was found to be similar to the value of latewood tracheid (1.72). The earlywood showed high anisotropic, its T/R shrinkage ratio was 2.75. The macroscopic shrinkage was the result of the interaction of the tracheids of earlywood and latewood and was mainly dominated by latewood tracheids.

The surface checks or internal cracks from drying could significantly affect the processing and utilization of the wood. Therefore, it is of great significance to investigate the formation mechanism of cracks and reduce its occurrence. In this work, the development of cracking was quantified and its relationship with moisture content (MC) gradient and anisotropic shrinkage was analyzed. Results showed that the slight shrinkage occurred at the MC of 40%, and the shrinkage ratio at the end of drying was about 7.38% in the tangential (T) direction and 4.35% in the radial (R) direction. The shrinkage ratio of T/R in the MC range of 30%–15% was about 1.8, which was higher than that (1.65) in the MC range of 15%–5%. Cracks initiation was observed at average MC of 45%. The area and number of cracks reached a maximum at 15% MC. During the late stage of drying, the drying stress of the surface layer was reversed from tensile to compressive, which leads to the narrowing or closure of the cracks. Moreover, the fracture morphology of wood cells was observed at the microscopic level, indicating that the failure firstly occurred in the intercellular layer between the ray tissue and the tracheid in the latewood. The ray cells presented intact, and the lamellar structure between ray tissues and between the ray cells and the tracheids were the weak points of wood during drying. The results would contribute to keeping in minimum drying defects and improving the drying quality of wood.

The effects of drying methods on equilibrated moisture content (MC) and swelling efficiency of Chinese cedar (Cryptomeria fortunei) wood were studied in this paper. Drying experiments were conducted with conventional (CON) drying and superheated steam (SHS) drying under atmospheric pressure. Specimens were equilibrated at two environment conditions to measure moisture and dimensional changes, and then the moisture excluding efficiency (MEE) and antiswelling efficiency (ASE) were determined. Results showed that the equilibrated MC of artificial-dried wood was lower than control samples (air drying), and the equilibrated MC of wood with SHS drying was lower than that with CON drying, which indicated that MEE was enhanced in SHS drying process. Similar results were found in swelling efficiency and ASE of artificial-dried wood and the control. The mechanism was studied by dynamic mechanical analysis (DMA) and X-ray diffraction analysis (XRD). The DMA results showed that both of relative storage modulus and relative loss modulus were the highest for SHS-dried wood and the lowest for the control samples. As for the crystalline structure assessed by changes of XRD, the results showed that the cellulose crystallinity and crystallite size of Chinese cedar wood with SHS drying were the highest, and control specimens were the lowest. All the analyses showed that Chinese cedar wood with low hygroscopic and high dimensional stability could be gotten through SHS drying process.

High-intensity microwave (HIMW) treatment is a time-saving and environmentally friendly method widely applied in the wood processing industry. It enhances wood permeability, making it suitable for drying and impregnation modification. This study aimed to investigate the effects of HIMW on macroscopic and microscopic cracks, tracheid cell wall damage, and the chemical structure of Chinese fir [Cunninghamia lanceolata (Lamb.) Hook] wood. Through the use of a camera, optical microscope, scanning electron microscope, transmission electron microscope, Fourier-transform infrared spectroscopy, and X-ray diffraction, the morphology of cracks, cell wall damage, the chemical composition of the cell wall, and the crystalline structure of cellulose treated with HIMW were examined and analyzed. The results revealed that the initial moisture content (MC) and microwave energy density (MWED) significantly influenced the crack characteristics and cell wall structure and slightly influenced the chemical composition and crystalline structure of cellulose of the Chinese fir cell wall. HIMW treatment can produce different characteristics of wood cracks. The size and number of cracks were significantly increased with the increase in MWED, and more cracks were found in low MC. Microcracks caused by HIMW treatment tended to initiate at the ray parenchyma, resulting in the stripping of ray cells along its radial direction. Meanwhile, the cracking of adjacent cell junctions, the rupturing of the pit margo and pit torus, and cell wall parts tearing along the direction of microfibers occurred as a result of the HIMW treatment. The most severe damage to the cell walls occurred at the interface of S1/S2, S1, and ML layers, and the cell walls were torn in the S2 layer. There were no significant changes in the FTIR spectra of the HIMW treatment samples. Hemicellulose degradation occurred first, which increased with the increase in MWED. The recrystallization of cellulose and the lignin content increased because of the change in the aromatic C=O groups. As MWED increased, both the crystallinity index (CI) and cellulose crystal width (D₂₀₀) of the samples that underwent HIMW treatment increased accordingly, and the number of low-MC samples was greater than that of the high-MC samples. The findings contribute to understanding the crack characteristics and damage mechanism induced by HIMW treatment on wood. This study provides valuable insights into regulating the effects of HIMW treatment and expanding its application in wood processing, such as wood drying and functionalized impregnation, according to the specific end-use requirements.