The technology currently used for the fabrication of toothed wheels, gear couplings and chain drums involves the induction hardening process or hardening and tempering after carburising. All these processes take a long time and cause adverse changes in the dimensions and surface quality of products, requiring post-treatment machining to remove the resulting cavities. The paper proposes the implementation of gear elements made of ductile iron with nanoausferritic matrix obtained by a new appropriate heat treatment process. The new material offers good performance characteristics and nearly no need for the application of other technological processes commonly used in the manufacture of gears.
1 April 2015 in Archives of Metallurgy and Materials
The aim of the study was to investigate the thermal stability of the nanostructure produced in X37CrMoV5-1 tool steel by austempering heat treatment consisted of austenitization and isothermal quenching at the range of the bainitic transformation. The nanostructure was composed of bainitic ferrite plates of nanometric thickness separated by thin layers of retained austenite. It was revealed, that the annealing at the temperature higher than temperature of austempering led to formation of cementite precipitations. At the initial stage of annealing cementite precipitations occurred in the interfaces between ferritic bainite and austenite. With increasing temperature of annealing, the volume fraction and size of cementite precipitations also increased. Simultaneously fine spherical Fe7C3carbides appeared. At the highest annealing temperature the large, spherical Fe7C3carbides as well as cementite precipitates inside the ferrite grains were observed. Moreover the volume fraction of bainitic ferrite and of freshly formed martensite increased in steel as a result of retained austenite transformation during cooling down to room temperature.
1 April 2015 in Archives of Metallurgy and Materials
The paper describes a comparative study of the corrosion resistance of bearing steel 67SiMnCr6-6-4 after two kinds of nanostructuring treatments and two kinds of conventional quenching and tempering treatments. The nanostructuring treatment consisted of austempering with an isothermal quenching at 240°C and 300°C. The conventional heat treatment consisted on quenching and tempering at 350°C for 1 h and quenching and tempering at 550°C for 1 h. Time and temperature of tempering was chosen so that the hardness of both samples (nanostructured as well as quenched and tempered) was similar. The microstructure of steel after each heat treatment was described with the use of transmission electron microscopy (TEM). It was shown, that the austempering conducted at 240°C produced homogenous nanobainitic structure consisting of carbide-free bainite plates with nanometric thickness separated by the layers of retained austenite. The austempering at 300°C produced a sub-micrometric carbide-free bainite with retained austenite in form of layers and small blocks. The conventional heat treatments led to a tempered martensite microstructure. The corrosion resistance study was carried out in Na2SO4acidic and neutral environment using potentiodynamic and electrochemical impedance spectroscopy (EIS) methods. The corrosion resistance of nanostructured steel samples were compared to the steel samples with tempered martensite. The obtained results indicate, that the corrosion resistance of bearing steel with nanobainitic structure is similar to steel with tempered martensite in both acidic and neutral environment. This means that the high density of intercrystalline boundaries in nanobinite does not deteriorate the corrosion properties of the bearing steel.
Identification of changes occurring on the working surface of lubricated gears using analytical equipment, e.g., an FE-SEM scanning electron microscope with an EDS microanalyzer, a WLI interferometric microscope, or a GDEOS optical discharge spectrometer, enables the characterisation of wear mechanisms of this surface. Definition of the phenomena occurring on the surface of tribo-couples after scuffing tests enables a comparative analysis of scuffing resistance and surface properties of the micro- and nanostructure, and elemental composition of the tested gears. Recognition and analysis of the wear mechanisms occurring on the working surface of gears will reduce the risk of damage and losses resulting from the need for maintenance and repair. The study concerned the working surfaces of gears made of 17HNM and 35HGSA steels on which a W-DLC/CrN coating was deposited. Shell Omala S4 GX 320 commercial industrial oil with a synthetic PAO (polyalphaolefin) base was selected for the lubrication of the gears. Tribological tests employed an FZG gear scuffing under severe conditions test method and they were carried out on a T-12U test rig for cylindrical gear analysis.