Thermal ionization mass spectrometry (TIMS) can provide highly accurate strontium (Sr), neodymium (Nd), and lead (Pb) isotope measurements for geological and environmental samples. Traces of these isotopes are useful for understanding crustal reworking and growth. In this study, we conducted a sequential separation of Sr, Nd, and Pb and subsequently measured the ⁸⁷Sr/⁸⁶Sr, ¹⁴³Nd/¹⁴⁴Nd, ²⁰⁶Pb/²⁰⁴Pb, ²⁰⁷Pb/²⁰⁴Pb, and ²⁰⁸Pb/²⁰⁴Pb ratios of 13 widely used rock certified reference materials (CRMs), namely BCR-2, BHVO-2, GSP-2, JG-1a, HISS-1, JLk-1, JSd-1, JSd-2, JSd-3, LKSD-1, MAG-1, SGR-1, and 4353A, using TIMS. In particular, we reported the first isotopic ratios of Sr, Nd, and Pb in 4353A, Sr and Nd in HISS-1 and SGR-1, and Sr in JLk-1, JSd-2, JSd-3, and LKSD-1. The Sr–Nd–Pb isotopic compositions of most in-house CRMs were indistinguishable from previously reported values, although the Sr and Pb isotopic ratios of GSP-2, JSd-2, JSd-3, and LKSD-1 obtained in different aliquots and/or batches varied slightly. Hence, these rock reference materials can be used for monitoring the sample accuracy and assessing the quality of Sr–Nd–Pb isotope analyses.

The Pirrit Hills are located in the Ellsworth–Whitmore Mountains of West Antarctica. The Pirrit Hills granite exhibits significant negative Eu anomalies (Eu/Eu* = 0.01~0.25) and a REE tetrad effect indicating intensive magmatic differentiation. Whole-rock Rb-Sr and Sm-Nd geochronologic analysis of the Pirrit Hills granite gave respective ages of 172.8 ± 2.4 Ma with initial ⁸⁷Sr/⁸⁶Sr = 0.7065 ± 0.0087 Ma and 169 ± 12 Ma with initial ¹⁴⁴Nd/¹⁴³Nd = 0.512207 ± 0.000017. The isotopic ratio data indicate that the Pirrit Hills granite formed by the remelting of Mesoproterozoic mantle-derived crustal materials. Both chondrite-normalized REE patterns and Sr-Nd isotopic data indicate that the Pirrit Hills granite has geochemical features of chondrite-normalized REE patterns indicating that REE tetrad effects and negative Eu anomalies in the highly fractionated granites were produced from magmatic differentiation under the magmatic-hydrothermal transition system.