Due to its outstanding electrical characteristics, such as the low temperature expansion coefficient, low dielectric constant and good mechanical properties, cordierite, 2MgO⋅2Al2O3⋅ 5SiO2, is a very attractive high-temperature ceramic material. In order to accelerate the process of sintering, 2.50 mass% Bi2O3 has been added to the starting mixtures. Liquid phase sintering caused by the presence of bismuth-oxide lowers the temperature of cordierite formation. The mechanical activation of the starting mixtures (0–56 min in vibro-mill) additionally lowers sintering temperatures. The sintering process was performed at 1200, 1300, 1350 and 1400 °C, for 2 h. The particle size analysis (PSA) was employed in order to determine the changes in the particle size of the mechanically treated powders. The phase composition of the starting powders and sintered materials was analyzed by the X-ray diffraction method. Furthermore, scanning electron microscopy (SEM) was used in the analysis of the powder morphology
In this study, polyvinyl alcohol (PVA) nanofibers with ethyl vanillin as an active compound were prepared using electrospinning technique. The final products of electrospinning process were in the form of nanofibers films. PVA/ethyl vanillin nanofibers, having fibers diameters in the range 100–1700 nm, were successfully electrospun from ethanol/water mixture of PVA and ethyl vanillin. The effects of immobilization process on ethyl vanillin thermal properties were investigated by differential scanning calorimetry (DSC). The results of DSC showed significant influence of immobilization process on thermal properties of ethyl vanillin. It was noticed that melting point of immobilized ethyl vanillin was lower (~55 °C) compared to free flavor (~77 °C). Our results showed that films based on PVA/ethyl vanillin nanofibers are mechanically stable.