This work addresses the two great challenges of the spark plasma sintering (SPS) process: The sintering of complex shapes and the simultaneous production of multiple parts. A new controllable interface method is employed to concurrently consolidate two nickel gear shapes by SPS. A graphite deformable sub-mold is specifically designed for the mutual densification of both complex parts in a unique 40 mm powder deformation space. An energy efficient SPS configuration is developed to allow the sintering of a large-scale powder assembly under electric current lower than 900 A. The stability of the developed process is studied by electro-thermal-mechanical (ETM) simulation. The ETM simulation reveals that homogeneous densification conditions can be attained by inserting an alumina powder at the sample/punches interfaces, enabling the energy efficient heating and the thermal confinement of the nickel powder. Finally, the feasibility of the fabrication of the two near net shape gears with a very homogeneous microstructure is demonstrated.

Spark Plasma Sintering (SPS) is used to fabricate Titanium-Niobium-Zirconium-Tantalum alloy (TNZT) powder—based bioimplant components with controllable porosity. The developed densification maps show the effects of final SPS temperature, pressure, holding time, and initial particle size on final sample relative density. Correlations between the final sample density and mechanical properties of the fabricated TNZT components are also investigated and microstructural analysis of the processed material is conducted. A densification model is proposed and used to calculate the TNZT alloy creep activation energy. The obtained experimental data can be utilized for the optimized fabrication of TNZT components with specific microstructural and mechanical properties suitable for biomedical applications.

Purpose: This study aims to provide understanding of the influence of external factors, such as gravity, during sintering of three dimensional (3D)-printed parts in which the initial relative density and cohesion between the powder particles are lower compared with those present in the green parts produced by traditional powder technologies. A developed model is used to predict shrinkage and shape distortion of 3D-printed powder components at high sintering temperatures. Design/methodology/approach: Three cylindrical shape connector geometries are designed, including horizontal and vertical tubes of different sizes. Several samples are manufactured by binder jetting to validate the model, and numerical results are compared with the measurements of the sintered shape. Findings: Simulations are consistent with empirical data, proving that the continuum theory of sintering can effectively predict sintering deformation in additively manufactured products. Originality/value: This work includes the assessment of the accuracy and limits of a multiphysics continuum mechanics–based sintering model in predicting gravity-induced distortions in complex-shaped additively manufactured components.