During the last several years, new multi- and single-layered archaeological sites, in which the most ancient Neolithic pottery in the Eastern Europe had been found, were excavated in the region of Lower Volga. Animal bones and organic materials were sampled from these sites for radiocarbon (14C) dating and diet investigations. The evidence from these studies suggests that the first domestic animals in the Lower Volga region appeared in the Cis-Caspian culture of the Early Eneolithic. Lipid analysis of food crusts from pottery allowed the cooked food to be characterized. The detailed chronology from Neolithic (6500–5400 cal BC) to Eneolithic (5300–4700 cal BC) cultures, as well as the diet of these ancient people, were reconstructed.
The unique archaeological monument of Okhta 1 (Neolithic-Early Metal Age) was excavated in 2008 in central Saint Petersburg (Russia). Radiocarbon and wiggle-match dating of organic materials and artifacts (charcoal wood samples and ceramic food crusts) from lithological and cultural layers helped to determine the main stages of cultural-historical processes and paleogeographical events in the coastal zone of the Baltic Sea bay during the Holocene. Humans occupied the Okhta Cape from 4200–3600 cal BC, after the Littorina Sea regression. Prehistoric people of the Middle-Late Neolithic, identified by their characteristic Pit Combed Ware ceramics, used this territory for fishing and hunting. The wood pile constructions used for fishing in 3500 cal BC were built on the coast and in river channels. From 3200–3000 cal BC, settlements and burials appeared of the Late Neolithic-Early Metal Age. The strategic geographical position of this territory was favorable for trade activity, fishing, and hunting, and shaped important interactions for different cultural groups.