Dissimilar Al/steel butt joints of 6.0 mm thick plates have been achieved using fiber laser keyhole welding autogenously. The cross sections, interface microstructures, hardness and tensile properties of Al/steel butt joints obtained under different travel speeds and laser beam offsets were investigated. The phase morphology and thickness of the intermetallic compound (IMC) layers at the interface were analyzed by scanning electronic microscopes (SEM) using the energy-dispersive spectrometry (EDS) and electron back-scattered diffraction (EBSD) techniques. The results show that travel speeds and laser beam offsets are of considerable importance for the weld shape, morphology and thickness of IMC layers, and ultimate tensile strength (UTS) of Al/steel butt joints. This proves that the IMC layers consist of Fe2Al5 phases and Fe4Al13 phases by EBSD phase mapping. Increasing laser beam offsets from 0.3 mm to 0.7 mm significantly decreases the quantity of Fe4Al13 phases and the thickness of Fe2Al5 layers at the interface. During tensile processing, the Fe2Al5 layer with the weakest bonding strength is the most brittle region at the interface. However, an intergranular fracture that occurred at Fe2Al5 layers leads to a relatively high UTS of Al/steel butt joints.
4 February 2016 in Industrial & Engineering Chemistry Research
Titanium-tantalum (Ti-Ta) alloy has excellent biomechanical properties with high strength and low Young’s modulus, showing great application potential in the biomedical industry. In this study, Ti-Ta alloy samples were prepared by laser powder bed fusion (LPBF) technology with mixed pure 75 wt.% Ti and 25 wt.% Ta powders as the feedstock. The maximum relative density of Ti-Ta samples prepared by LPBF reached 99.9%. It is well-accepted that four nonequilibrium phases, namely, α′, α″ and metastable β phase exist in Ti-Ta alloys. The structure of α′, α″ and β are hexagonal close-packed (HCP), base-centered orthorhombic (BCO) and body-centered cubic (BCC), respectively. X-ray Diffraction (XRD) analysis showed that the α′ phase transformed to the α″ phase with the increase of energy density. The lamellar α′/α″ phases and the α″ twins were generated in the prior β phase. The microstructure and mechanical properties of the Ti-Ta alloy were optimized with different LPBF processing parameters. The samples prepared by LPBF energy density of 381 J/mm3 had a favorable ultimate strength (UTS) of 1076 ± 2 MPa and yield strength of 795 ± 16 MPa. The samples prepared by LPBF energy density of 76 had excellent ductility, with an elongation of 31% at fracture.