Metallic material concepts associated with the sustainable and efficient use of resources are currently the subject of intensive research. Al addition to steel offers advantages in view of lightweight, durability, and efficient use of high-Fe scrap from the Al industry. In the present work, Al was added to Fe-12Cr-(9,12)Ni-3Mn-0.3C-xAl (x = 0.1–6) (wt.%) stainless steels to assess its influence on microstructure and mechanical properties. According to density measurements based on Archimedes’ principle, densities were between 7.70 and 7.08 g/cm3. High-energy X-ray diffraction estimations of the lattice parameter indicated that nearly 31% of density reduction was caused by the lattice expansion associated with Al addition. Depending on Al concentration, austenitic and duplex matrix microstructures were obtained at room temperature. In the presence of up to 3 wt.% Al, the microstructure remained austenitic. At the same time, strength and hardness were slightly enhanced. Al addition in higher quantities resulted in the formation of duplex matrix microstructures with enhanced yield strength but reduced ductility compared to the austenitic alloys. Due to the ready formation of B2-(Ni,Fe)Al intermetallics in the ferrite phase of the present alloy system, the increase in strength due to the presence of ferrite was more pronounced compared to standard duplex stainless steels. The occurrence of B2 intermetallics was implied by dilatometry measurements and confirmed by electron microscopy examinations and high-energy X-ray diffraction measurements.
22 August 2023 in International Journal of Fatigue
Additive manufacturing (AM) processes such as electron beam melting (EBM) are characterized by unprecedented design freedom. Topology optimization and design of the microstructure of metallic materials are enabled by rapid progress in this field. The latter is of highest importance as many applications demand appropriate mechanical as well as functional material properties. For instance, biodegradable implants have to meet mechanical properties of human bone and at the same time guarantee adequate cytocompatibility and degradation rate. In this field, pure iron has come into focus in recent studies due to its low toxicity. Hierarchical microstructures resulting from the EBM solidification processes and intrinsic heat treatment, respectively, allow for an adjustment of the degradation behavior and may promote enhanced fatigue strength. Herein, commercially pure iron (cp‐Fe) is processed by EBM. Microstructural analysis as well as an evaluation of the cyclic mechanical material properties are conducted. The results are compared to a hot‐rolled (HR) reference material. A contradiction observed as the EBM‐processed cp‐Fe (EBM Fe) shows lower ultimate tensile strength under monotonic loading but improved fatigue properties compared to the HR Fe. It is revealed that such a unique behavior originates from prevailing microstructural features in the EBM as‐built condition.
The complex thermal history imposed by the laser-based powder bed fusion of metals (PBF-LB/M) process is known to promote the evolution of unique microstructures. In the present study, metastable CrMnNi steels with different nickel contents and, thus, different phase stabilities are manufactured by PBF-LB/M. Results clearly reveal that an adequate choice of materials will allow to tailor mechanical properties as well as residual stress states in the as-built material to eventually redundantize any thermal post-treatment. The chemical differences lead to different phase constitutions in as-built conditions and, thus, affect microstructure evolution and elementary deformation mechanisms upon deformation, i.e., twinning and martensitic transformation. Such alloys designed for additive manufacturing (AM) highlight the possibility to tackle well-known challenges in AM such as limited damage tolerance, porosity and detrimental residual stress states without conducting any post treatments, e.g., stress relieve and hot isostatic pressing. From the perspective of robust design of AM components, indeed it seems to be a very effective approach to adapt the material to the process characteristics of AM.