High-photoluminescence (PL) graphene quantum dots (GQDs) were synthesized by a simple one-pot hydrothermal process, then separated by dialysis bags of different molecular weights. Four separated GQDs of varying sizes were obtained and displayed different PL intensities. With the decreasing size of separated GQDs, the intensity of the emission peak becomes much stronger. Finally, the GQDs of the smallest size revealed the most energetic PL intensity in four separated GQDs. The PL energy of all the separated GQDs shifted slightly, supported by density functional theory calculations.

In this paper, a novel phosphorus-doped sulfur quantum dots (P-SQDs) material was prepared using a simple hydrothermal method. P-SQDs have a narrow particle size distribution as well as an excellent electron transfer rate and optical properties. Compositing P-SQDs with graphitic carbon nitride (g-C₃N₄) can be used for photocatalytic degradation of organic dyes under visible light. More active sites, a narrower band gap, and stronger photocurrent are obtained after introducing P-SQDs into g-C₃N₄, thus promoting its photocatalytic efficiency by as much as 3.9 times. The excellent photocatalytic activity and reusability of P-SQDs/g-C₃N₄ are prospective signs of its photocatalytic application under visible light.

Photocatalysis holds great promise for addressing water pollution caused by organic dyes, and the development of Ag₂O/Fe₃O₄ aims to overcome the challenges of slow degradation efficiency and difficult recovery of photocatalysts. In this study, we present a novel, environmentally friendly Ag₂O/Fe₃O₄ magnetic nanocomposite synthesized via a simple coprecipitation method, which not only constructs a type II heterojunction but also successfully couples photocatalysis and Fenton reaction, enhancing the broad-spectrum response and efficiency. The Ag₂O/Fe₃O₄ (10%) nanocomposite demonstrates exceptional degradation performance toward organic dyes, achieving 99.5% degradation of 10 mg/L methyl orange (MO) within 15 min under visible light irradiation and proving its wide applicability by efficiently degrading various dyes while maintaining high stability over multiple testing cycles. Magnetic testing further highlighted the ease of Ag₂O/Fe₃O₄ (10%) recovery using magnetic force. This innovative approach offers a promising strategy for constructing high-performance photocatalytic systems for addressing water pollution caused by organic dyes.