Large composite structures manufactured out-of-autoclave require the assembly and bonding of multiple parts. A one-shot cure manufacturing method is demonstrated using powder epoxy. Lap shear plates were manufactured from powder epoxy and glass fiber-reinforced plastic with four different bonding cases were assessed: secondary bonding using standard adhesive film, secondary bonding using powder epoxy, co-curing, and co-curing plus a novel Z-pinning method. This work investigates the lap shear strength of the four cases in accordance with ISO 4587:2003. Damage mechanisms and fracture behavior were explored using digital image correlation (DIC) and scanning electron microscopy (SEM), respectively. VTFA400 adhesive had a load at break 24.8% lower than secondary bonding using powder epoxy. Co-curing increased the load at break by 7.8% compared to powder epoxy secondary bonding, with the co-cured and pinned joint resulting in a 45.4% increase. In the co-cured and co-cured plus pinned cases, DIC indicated premature failure due to resin spew. SEM indicated shear failure of resin areas and a large amount of fiber pullout in both these cases, with pinning delaying fracture phenomena resulting in increased lap joint strength. This highlights the potential of powder epoxy for the co-curing of large composite structures out-of-autoclave.
8 August 2022 in Plastics, Rubber and Composites: Macromolecular Engineering
This work discusses the development and refinement of a polymer/fibre through thickness reinforcement method. Similar in initial concept to the traditional metalworking process of riveting this allows the manufacture of through thickness reinforced 2-D preforms. Pins are placed with deliberate excess length using a veterinary needle to part in-plane fibres. A lay-up with an array of pins is then subjected to a hot-press process flattening the pin ends resulting in a consolidated preform. This preform exhibits useful characteristics such as the ability to be cut and reformed to a new topology, with the through thickness reinforcement also conforming to the new shape. Refinements to the process introduce a multi-stage press process aimed at improving pin orientation with both original and refined processes evaluated using ASTM D5528 to determine the effect on interlaminar fracture toughness.