This study investigated the impact of sonication parameters on the efficiency of the extraction of bioactive substances from hawthorn berries. The ultrasonic treatment was performed in two modes: continuous and pulse. In the pulse mode, the samples were sonicated with the following processor settings: 1 s on-2 s off. The effective ultrasonic processor times were 5, 10, and 15 min, and the total extraction times were 15 min, 30 min, and 45 min. The content of total polyphenols and total anthocyanins was determined by a spectrophotometric method. We show that the operating mode of the processor affects extraction efficiency, energy consumption and unit energy inputs. Extraction supported by a pulsating ultrasonic field allowed saving from 20% to 51% of energy with a simultaneous higher efficiency of the process. In addition, we show that the unit energy consumption in the pulsed mode was about 40% to 68% lower than the energy consumption in the case of continuous operation.

This study investigated the effects of particle size and ultrasonic parameters on the yields of bioactive compounds extracted from the leaves and inflorescences of hemp. The total flavonoid and anthocyanin contents were determined using the spectrophotometric method. The response surface methodology (RMS) was employed to optimize the yield of bioactive substances. On the basis of the developed model, the highest flavonoid yield was obtained under the following extraction conditions: particle size, 0.59 mm; extraction time, 10.71 min; ultrasound intensity, 7.13 W∙cm⁻²; extraction yield, 9.28 mg QE∙g⁻¹; determination coefficient, R² = 0.97. The optimal conditions for extracting anthocyanins were as follows: particle size, 0.25 mm; extraction time, 15 min; ultrasound intensity, 8.60 W∙cm⁻²; extraction efficiency, 20.27 mg Cy-GE∙100 g⁻¹; determination coefficient, R² = 0.87. This study helped confirm the importance of pulsed ultrasound-assisted extraction in obtaining bioactive compounds from hemp.

The purpose of this study was to determine the impact of the pomace drying methods (freeze-drying and convection-drying) and their percentage (0–10%) on selected physicochemical properties of gluten-free bread. The contents of nutrients (protein, fiber, fat, ash, and carbohydrates), bioactive compounds, antioxidant properties, acidity, baking efficiency, and moisture of the obtained products were determined. Fortifying the bread with raspberry pomace resulted in a change in fiber content from 18.13% d. b. (control sample) up to 19.97% d. b. (10% of freeze-dried pomace), and a change in the fat and ash content in the bread from 5.74% and 2.83% d. b. (control sample) to 7.18% and 3.12% d. b. (10% of freeze-dried pomace). The content of carbohydrates decreased after adding raspberry pomace to the bread, from 65.71% d. b. (control sample) to 63.68% d. b. (5% of freeze-dried pomace). The research carried out also showed that the introduction of 10% freeze-dried raspberry pomace increased the total polyphenol content by 81.75% and the antioxidant properties defined by the ABTS method by 159.54% and by the DPPH method by 96.43% compared to the control bread. The introduction of pomace resulted in a significant reduction in the total baking loss, from 15.1% to 10.62%, and an increase in the total titratable acidity of the crumb, from 2.13 mL _NaOH/10 g d. b to 7.78 mL _NaOH/10 g d. b. Principal component analysis highlighted a marked effect of the drying method and content of raspberry pomace on the quality values of gluten-free bread. This research demonstrated that raspberry pomace can be a valuable source of fiber and bioactive substances in gluten-free bread.

The aim of the study was to assess the effect of adding convectively dried and freeze dried raspberry and chokeberry pomace on the color (CIELab color space), texture (TPA test) and sensory evaluation (5-point scale) of gluten-free bread. Only in the case of bread with 10% addition of convectively dried chokeberry pomace, no statistically significant changes in color parameters were noted after baking and after 24 h. The highest increase in the lightness value (L*) (by 10.38%) was noted for gluten-free bread with 10% addition of freeze dried raspberry pomace, while the lowest (by 1.70%) was noted for bread with 5% addition of freeze dried raspberry pomace. In the case of enrichment of bread with chokeberry pomace, the highest increase in value (by 27.09%) was noted for bread with 10% addition of freeze dried chokeberry pomace, and the lowest (by 4.33%) for the control bread. The addition of raspberry pomace had no significant effect on the hardness and elasticity of the bread, but significantly reduced the cohesiveness of the crumb. The highest increase in hardness, by 95.9% compared to fresh bread, was observed for sample bread with 10% convection dried raspberry pomace addition (10CD_R). The introduction of raspberry pomace to the recipe did not significantly affect the chewiness of the bread, except for the sample with 10% addition of freeze dried pomace. In most cases, no significant increase in the chewiness of bread stored for 24 h was observed compared to fresh bread. In the case of chokeberry pomace, its addition did not cause significant changes in the elasticity and cohesiveness of the crumb, but a decrease in hardness and chewiness was noted. In the sensory assessment, the most tasty bread was considered to be the one with 10% addition of freeze dried raspberry pomace, while the least tasty bread was considered to be the one without raspberry and chokeberry pomace. The highest average of all parameter ratings was obtained by bread samples with a 5% addition of convection dried chokeberry pomace (5CD_C) (3.68).Gluten-free breads containing chokeberry and raspberry pomace could be implemented in bakery production, as they are accepted by consumers, but it is advisable to conduct further research on extending their shelf life.

The purpose of this study was to optimize the effect of particle size, time and ultrasonic intensity on the extraction of phenolic compounds and energy efficiency. Sonication was performed with a VC750 Sonics processor at the following amplitudes: 30, 50 and 70%, which corresponds to the ultrasonic intensity, respectively: 1.6; 5.1 and 8.6 W∙cm⁻². The frequency of ultrasound was 20 kHz. Extraction was carried out in a 5 s on–10 s off pulse system. The content of polyphenols and their antioxidant activity were assayed by the spectrophotometric method. Response surface methodology (RMS) was used to optimize the investigated variables. On the basis of the developed model, the highest polyphenols yield was obtained under the following extraction conditions (particle size 0.65 mm, extraction time 13.14 min, ultrasound intensity 6.92 W∙cm⁻², which resulted in a maximum value of 15.24 mg GAE∙g⁻¹ dry matter of hemp. Taking into account the lowest unit energy consumption, the best conditions were obtained for particle size of approx. 0.5 mm, extraction time 7.7 min, and ultrasound intensity 1.8 W∙cm⁻², which resulted in a phenolic yield of 10.14 mg GAE∙g⁻¹ dry matter of hemp. The best agreement between values of optimization variables within investigated criteria was obtained for the variable particle size. The developed models of pulsed ultrasound-assisted extraction can be used for obtaining polyphenols from Cannabis sativa L. at low unit energy consumption.

Hemp inflorescences from byproducts have been proposed as an addition to gluten-free rice bread. The scope of the research was to bake a control loaf of bread as well as bread loaves containing 1%, 2%, 3%, 4%, and 5% dried and crushed hemp inflorescence (HI). The loaves of bread were evaluated in terms of their physical and sensory properties, polyphenol and flavonoid contents, and DPPH and FRAP antioxidant activities. The study’s findings revealed that the addition of HI influenced changes in the physical properties of the bread loaves, such as increased specific volume, decreased bread hardness, increased elasticity, and chewiness of the breadcrumb, especially when the additive concentrations were greater than 3%. The addition of HI significantly increased the total amount of polyphenols, flavonoids, and antioxidant activity in the bread. The sensory evaluation revealed that gluten-free bread can be produced with a maximum of 2% HI without affecting its taste and aroma.