Post-bond heat treatment (PBHT) is an effective way to improve the bonding quality of a brazed joint. Herein, brazing of a nickel-based single crystal superalloy is carried out using a Ni-Cr-Co-B-Si-Al-Ti-W-Mo filler alloy, and the microstructure and creep property of the brazed joint are systematically investigated using scanning electron microscopy (SEM), Thermo-Calc software, an electron probe micro-analyzer (EPMA), X-ray diffractometer, confocal scanning laser microscope (CSLM), and transmission electron microscopy (TEM). The results reveal that the as-prepared joint only consists of an isothermally solidified zone (ISZ) and an athermally solidified zone (ASZ), where the cubic γ′ phase is observed in the ISZ, and skeleton-like M₃B₂, γ + γ′ eutectic and reticular G phases are observed in the ASZ. Furthermore, the γ + γ′ eutectic and G phases disappear and the M₃B₂ alters from a skeleton-like to block-like shape in the ASZ after PBHT. Meanwhile, some lath-like M₃B₂ phases are precipitated at the edge of the ISZ and several M₃B₂ phases are precipitated in the base metal, forming a new zone in the brazed joint, namely at the diffusion affected zone (DAZ). Owing to the removal of low melting point eutectics from the as-prepared joint, the creep life also increases from 188 h to 243 h after PBHT. The current work provides a method for the optimization of brazed joints based on the Ni-based single crystal superalloy.

In order to meet the demand for high wear-resistant Co-based material used in fields such as aerospace, energy, medical, etc., this study attempts to improve the comprehensive performance of this material by adding some reinforced phases and adjusting the sintering temperature. Results indicate the pure Co–Cr–W alloy is composed of γ-Co, M₂₉C, and M₆C (Ni₃W₃C), and the Co–Cr–W matrix composites are composed of γ-Co, M₂₉C, M₆C (Co₂W₄C), M₂₃C₆, and WC. With increasing the hot-pressing sintering temperature, the element diffusion in the material becomes sufficient, and the microstructure of Co–Cr–W alloy and composites materials becomes denser. When the sintering temperature is over 1150 °C, the bending strength and the toughness of the Co–Cr–W matrix composites are higher than that of the pure Co–Cr–W alloys. The added reinforced phases help the composites to gain a multi-scale strengthening effect, which makes the composites have a more comprehensive performance. Our results emphasize the importance of added reinforced phases and help to optimize the preparing process in preparing the Co–Cr–W alloys.