Microbial induced calcium carbonate precipitation (MICP) provides a theoretical basis for repairing underground rocks. The optimal germination conditions and mineralization activities of Bacillus pasteurii with crack repair function were investigated. The growth and mineralization properties of microorganisms in different environments were explored by measuring the urease activity and calcium carbonate production of bacteria, and the influencing factors of bacterial biomass and urease activity were analyzed. The microscopic morphology of bacterial mineralization products was analyzed by SEM, XRD and TG-DSC test. The influencing factors of spore germination rate were studied by measuring the OD value of spore germination. The results showed that under the conditions of pH 7.3, urea concentration 0.25–0.5 mol l−1, and calcium ion concentration 0.4–0.6 mol l−1, the mineralization activity of B. pasteurii was the strongest, and the generated mineralization product was a stable calcite crystal. The optimum concentration of germination agent and inorganic salt were 10 mmol l−1 and 200 mmol l−1, respectively.
This study investigated the mechanism, prevention measures, and control methods for earthquake disasters typically occurring in mines with thick and hard rock strata. A mine stope with large faults and thick hard rock strata in Hebei Province was taken as the background study object. Then, theoretical analysis and numerical simulation methods were adopted in conjunction with field monitoring to explore how horizontal stress evolves in the thick and hard hanging roofs of such mines, potentially leading to mining earthquakes. Then, based on the obtained results, a mining design method was proposed to reduce the horizontal stress levels of earthquake mitigation. The results showed that, under the control of large faults, semiopen and semiclosed stopes with thick hard rock strata are formed, which cause influentially pressurized and depressurized zones during the evolution of the overburden movements and horizontal stress. It was determined that the stress concentrations mainly originated from the release and transfer of horizontal stress during the rock fractures and movements in the roof areas, which were calculated using a theoretical estimation model. The horizontal stress concentrations formed “counter torques” at both ends of the thick and hard strata, which prevented the support ending due to tensile failures. As a result, the limit spans were increased. This study proposed a mining strategy of using narrow working faces, strip mining processes, and reasonable mining speeds, which could effectively reduce horizontal stress concentrations and consequently prevent and control mining earthquakes. This study’s research results were successfully applied to the mining practices in working face 16103.
To study the influence of cyclic disturbance stress on the mechanical behavior of coal during mining, a gas containing coal fluid-solid coupling servo seepage experimental system was used to conduct experimental research on the acoustic emission (AE) characteristics of gas containing coal under two stress paths of graded cyclic loading and unloading. The AE characteristics of coal damage and failure processes under different cyclic stress paths were analyzed. The research results indicate that: (1) The overall characteristics of AE signals for both graded cyclic loading and unloading paths are basically the same. With increasing of the amount of graded cyclic loading or unloading, the AE count reaches its maximum value when reaching failure, and the cumulative ringing calculation of AE increases exponentially. (2) The AE signals under the graded cyclic loading or unloading path exhibit obvious zoning characteristics. In the low and medium stress regions, the AE signal basically satisfies the Kaiser effect, while reaching the high stress region before failure, the AE signal exhibits a significant Felicity effect. (3) The concentration coefficient of AE and the intensity coefficient of the Kaiser effect have been newly defined. They are used to quantitatively characterize the extent of the Kaiser effect of AEs under graded cyclic stress. It was found that as the variation of graded cyclic stress increases, the concentration coefficient and Kaiser effect intensity coefficient both show a decreasing trend. (4) Combining the AF and RA values of AE, it was found that the coal failure signals of the two stress paths were basically similar, that is, the overall failure was mainly tensile failure, and the signals of cyclic unloading tensile failure were significantly more than those of cyclic loading. The AE signal characteristics studied in this article are of great significance for predicting coal power disasters.
Cracks in underground rock masses cause gas leakage, seepage, and water inflow. To realize calcium carbonate deposition and mineralization filling in rock cracks, microencapsulated bacterial spores were prepared by an oil phase separation method. To optimize the microorganism growth conditions, the effects of microcapsules with various pHs, particle sizes, and amounts on microcrack self-healing were investigated through an orthogonal test, and the best conditions for repairing the cracks using microencapsulated Bacillus sphaericus were obtained. Infrared analysis and scanning electron microscopy were used to observe the morphological characteristics and coating performance of the microcapsules. The results showed that the microcapsules contained functional groups in the core and wall materials. The surfaces of the microcapsules prepared by the test were rough, which was beneficial for adhesion onto the fracture surface. X-ray diffraction analysis, X-ray photoelectron spectroscopy, and thermal analysis were conducted. The results showed that the microcapsules with pH = 8 and a particle size of 100 μm had the highest thermal decomposition temperature and the best thermal stability. The elements of the core and wall materials were detected in the microcapsules, and the coating had a beneficial effect. The compression and acoustic emission tests of the specimens embedding microbial capsules with different contents under different working conditions revealed that the two fractures of the specimen were due to the rupture of the microcapsule and the rupture of the rock specimen, indicating the best mechanical triggering properties and compressive properties of the microcapsule.
A dynamic coupled elastoplastic damage model for rock-like materials is proposed. The model takes unified strength theory as the strength criterion. To characterize the different damage between compression and tension, two damage variables both in compression and in tension are introduced into the model. The former is represented by the generalized shear plastic strain and volumetric plastic strain and the latter is expressed with the generalized shear plastic strain. Furthermore, the model takes the strain rate effect into account to reflect the strength enhancement under dynamic loading. Because of the difference in plastic hardening between compression and tension, a modified hardening function is adopted. At the same time, the volume strain from HJC model is modified to be consistent with one of continuum mechanics. The developed model is numerically implemented into LS-DYNA with a semi-implicit algorithm through a user-defined material interface (UMAT). The reliability and accuracy of the developed model are verified by the simulation of four basic experiments with different loading conditions. The proposed model was found to be applicable to different mechanical behaviors of rock-like materials under static and dynamic loading conditions.
1 January 2018 in Journal of the Southern African Institute of Mining and Metallurgy