Thermoplastic elastomer vulcanizate (TPV) and liquid silicone rubber (LSR) are replacement candidates for ethylene-propylene-diene rubbers (EPDM), as they offer the possibility for two-component injection moulding. In this study, these material types were compared side by side in cyclic compression tests. The materials were also characterized to provide details on the formulations. Compared to the rubbers, the TPV had higher compression set (after a given cycle) and hysteresis loss, and a stronger Mullins effect. This is due to the thermoplastic matrix in the TPV. The LSR had lower compression set (after a given cycle) than the EPDM, but stronger Mullins effect and higher relative hysteresis loss. These differences between the LSR and the EPDM are likely due to differences in polymer network structure and type of filler. Methods for quantifying the Mullins effect are proposed, and correlations between a Mullins index and parameters such as compression set are discussed. The EPDMs showed a distinct trend in compression set, relative hysteresis loss and relaxed stress fraction vs. strain amplitude; these entities were almost independent of strain amplitude in the range 15–35%, while they increased in this range for the TPV and the LSR. The difference between the compression set values of the LSR and the EPDM decreased with increasing strain amplitude and increasing strain recovery time.
1 January 2018 in Advances in Materials Science and Engineering
Improving the success rate in additive manufacturing and designing highly optimized structures require proper understanding of material behaviour. This study proposes a novel experimental method by which anisotropic mechanical properties of additively manufactured materials can be assessed. The procedure is based on tensile testing of flat specimens, manufactured by laser powder bed fusion (LPBF) at different orientations relative to the build plate. In this study, the procedure was applied to the Inconel 718 alloy. Three identical specimen sets were built, each of which received complementary postprocessing treatments. The tensile tests were carried out on specimens with as‐built surface finish. Digital image correlation was used to record the strain field evolution on two perpendicular surfaces of the tensile specimens under loading. An optimization algorithm is also proposed for determining the anisotropic elastic constants using only a few tensile test results. It was observed that both build orientation and postprocessing have strong influence on the anisotropic mechanical properties of the material. The effect of microstructure was also investigated and characterised. Consequently, three transversely isotropic compliance matrices were constructed, representing the effect of the different processing conditions.