Understanding the formation of the North Qilian Shan in the NE Tibetan Plateau provides insights into the growth mechanisms of the northern region of the plateau across time. Detrital zircon fission-track (ZFT) analyses of river sediments can provide a comprehensive understanding of the exhumation history during prolonged orogenesis. Here, we applied the detrital thermochronology approach to the Qilian Shan orogenic belt. This work presents the first single-grain detrital ZFT data from river-bed sediments of the upper Hei River catchment in North Qilian Shan. The single ZFT ages are widely distributed between about 1200 Ma and about 40 Ma. These data record the protracted history of the Qilian Shan region from the Neoproterozoic evolution of Rodinia and late Paleozoic amalgamation of Central Asia to the accretion of the Gondwanian blocks during the Meso-Cenozoic era. Strong post-magmatic cooling events occurred in North Qilian Shan at 1200~1000 Ma, corresponding to the assembly of the Rodinia supercontinent. The age population at 800 Ma documents the oceanic spreading in the late Neoproterozoic dismantling of Rodinia. ZFT ages ranging from about 750 Ma to 550 Ma (with age peaks at 723 Ma and 588 Ma) are consistent with the timing of the opening and spreading of the Qilian Ocean. The age peaks at 523 Ma and 450 Ma mark the progressive closure of that ocean ending with the collision of the Qilian block with the Alxa block—North China craton in the Devonian. The Qilian Ocean finally closed in Late Devonian (age peak at 375 Ma). In the late Paleozoic (275 Ma), the subduction of the Paleotethys Ocean led to extensive magmatic activity in the North Qilian Shan. During the Lower Cretaceous (145 Ma), the accretion of the Lhasa block to the south (and potentially the closure of the Mongol-Okhotsk Ocean to the northeast) triggered a renewed tectonic activity in the Qilian Shan. Finally, a poorly defined early Eocene exhumation event (50 Ma) suggests that the NE Tibetan Plateau started to deform nearly synchronously with the onset of the India-Asia collision. This study demonstrates the usefulness of combining modern-river detrital thermo-/geochronological ages and bedrock geochronological ages to understand large-scale orogenic evolution processes.

The Qinling Shan is located between the North China Craton and the South China Block. Not only is investigating the exhumation process of the Qinling Shan beneficial for comprehending the tectonic collision history of mainland China but also for enhancing our understanding of the development of the Yellow and Yangtze Rivers. Previous studies have predominantly focused on bedrock analysis in the Qinling Shan. However, modern fluvial detrital samples offer a more extensive range of thermal history information. Therefore, we gathered modern fluvial debris samples from the Hanjiang River, which is the largest river in the South Qinling Shan. Subsequently, we conducted apatite fission-track analysis using the laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) method. A total of 214 valid track ages were obtained, with an age distribution ranging from 9.5 to 334.0 Ma. The Density Plotter software was employed to decompose the data and generate four prominent age peaks: 185, 103, 69, 35, and 12 Ma. The exhumation events of the Early Jurassic (185 Ma) and Cretaceous (103–69 Ma) in the Southern Qinling Shan were strongly influenced by the collision between the South China Block and the North China Craton, as well as the subduction of the West Pacific Plate, respectively. The far-field effect of the collision between the Indian Plate and the southern Asian continent influenced the exhumation of the South Qinling Shan during the Late Eocene (35 Ma) and Middle Miocene (12 Ma), respectively. In conjunction with the reported findings, we comprehensively analyzed the geological implications of the Mesozoic and Cenozoic exhumations of the Qinling Shan. The Qinling Shan emerged as a watershed between the Ordos and Sichuan Basins in the early Mesozoic and Cenozoic, respectively. However, the exhumation and expansion of the Tibetan Plateau has forced the Yangtze River to flow eastward, resulting in its encounter with the South Qinling Shan in the late Cenozoic. The exhumation of the Qinling Shan has resulted in fault depression in the southern Ordos Basin. This geological process has also contributed to the widespread arid climatic conditions in the basin. During the Miocene, the Yellow River experienced limited connectivity due to a combination of structural and climatic factors. As a result, the Qinling Shan served as an obstacle, dividing the connected southern Yangtze River from the northern segment of the Yellow River during the late Cenozoic era.

The emergence of the Tibetan Plateau is one of the most significant geological events in East Asia. The Central Qilian Shan connects North and South Qilian Shan in the northeastern part of the Tibetan Plateau. However, the exhumation history of the Central Qilian Block from the Mesozoic to Cenozoic remains unclear. Determining the cooling ages of detrital zircon and apatite in modern river sediments is an ideal method for tracing the evolutionary processes of orogenic belts. In this study, we present the first single-grain detrital apatite (153) and zircon fission-track (108) data for the Huangshui River sediments from the Central Qilian Shan. The decomposition of the dataset revealed major Mesozoic and Cenozoic age peaks at ca. 145–93, and 11 Ma. The Central Qilian Shan entered the intracontinental orogeny stage dating back to the Cretaceous (ca. 145–93 Ma) and Late Cenozoic (ca. 11 Ma) caused by the subduction of the Neo-Tethys and Indian–Asian collision. Therefore, we propose that the geomorphic framework of the northeastern margin of the Tibetan Plateau was initially established during the Mesozoic and further consolidated in the Late Miocene.

Eolian sediments are extensively distributed across the Earth’s surface, and their formation is intricately linked to climate change, tectonic activity, and topographic features. Consequently, the investigation of eolian sediments bears great geological significance. The northwest region of China is renowned for hosting the most extensive and thickest Late Miocene–Pliocene red clay deposits globally. Nonetheless, scholars have yet to reach a consensus regarding the precise formation processes of these red clays. The identification of the source region of the red clays is crucial for comprehending their formation mechanism. The correlation of zircon U-Pb age spectra is a frequently utilized method for determining the provenance of eolian sediments. In this study, we compared the previously published zircon U-Pb ages (n = 12,918) of the Late Miocene–Pliocene red clays in the Ordos Plateau with those from the potential provenance regions (n = 24,280). The analysis, supported by the tectonic and climatic background of the region, revealed that the Late Miocene–Pliocene red clay in the Ordos Plateau originates predominantly from the Yellow and Wei rivers, with a minor contribution from the weathering of bedrock in the western North China Craton. The transport of these detrital materials by the East Asian winter monsoon is impeded by the presence of the Qinling and Taihang Shan, resulting in their deposition on the flat surface of the Ordos Plateau. This development of red clay is consistent with the proximal accumulation model, illustrating how the hydrosphere, atmosphere, and lithosphere interacted to shape the red clay deposits during the Late Miocene and Pliocene periods in the Ordos Plateau.

The Yellow River (~5464 km) and the Yangtze River (~6300 km) are large rivers that originate from the Tibetan Plateau and flow into the western Pacific Ocean. The shelf seas of the western Pacific Ocean (e.g., Bohai, Yellow, and East China seas) serve as critical sites for investigating the evolution of these rivers. Distinguishing the material signals of the Yellow River from those of the Yangtze River is an essential step in this research. Therefore, we analyzed published zircon U-Pb ages (n = 1568 for the Yellow River and n = 1216 for the Yangtze River) and K-feldspar Pb isotopes (n = 380 for the Yellow River and n = 158 for the Yangtze River) from the middle and lower reaches of both rivers. The results indicate that the detrital material in the lower reaches of the Yellow River is primarily influenced by the western North China Craton and the Qinling Mountains, whereas the detrital material in the lower reaches of the Yangtze River mainly derives from the South China Block. The Qinling Mountains influence the material composition of the lower Yellow River, primarily due to the formation of overhanging rivers along the river’s course. These geological features inhibit the inflow of materials from the eastern North China Craton, thereby preventing the mixing from the Qinling Mountains. In contrast, the influence of the Qinling Mountains on the material composition of the lower Yangtze River is minimal. This limited impact is attributed to the influx of materials from the South China Block, which dilutes the contributions from the Qinling Mountains. Notably, substantial discrepancies exist in the U-Pb ages and Pb isotopic compositions of detrital zircons and K-feldspar from the lower Yellow River compared to those from the lower Yangtze River and the surrounding geological units. These disparities provide a robust foundation for investigating large river provenance tracing in the western Pacific Ocean shelf sea through the integration of these two analytical methods. However, the U-Pb age distributions of detrital zircons in the lower Yellow River have changed significantly over geological time. The U-Pb age data for detrital zircons collected from the eastern Sanmen Gorge of the middle Yellow River should be utilized to examine river evolution prior to the Quaternary period. Conversely, the U-Pb data from detrital zircons in the lower Yellow and the Yiluo rivers should be considered when discussing Quaternary river evolution. The zircon U-Pb age characteristics of the lower Yangtze River can be directly employed to analyze the evolution of large rivers in the western Pacific Ocean shelf sea during the Neogene.