The symmetric zero-frequency mode induced by weak material nonlinearity during Lamb wave propagation is explored for the first time. We theoretically confirm that, unlike the second harmonic, phase-velocity matching is not required to generate the zero-frequency mode and its signal is stronger than those of the nonlinear harmonics conventionally used, for example, the second harmonic. Experimental and numerical verifications of this theoretical analysis are conducted for the primary S₀ mode wave propagating in an aluminum plate. The existence of a symmetric zero-frequency mode is of great significance, probably triggering a revolutionary progress in the field of non-destructive evaluation and structural health monitoring of the early-stage material nonlinearity based on the ultrasonic Lamb waves.

Ti matrix composites reinforced with 1–5 wt% graphene oxide (GO) were prepared by hot-pressed sintering in argon atmosphere. The effect of sintering temperature on the microstructures and mechanical properties of the composite was also evaluated. The results show that TiC nanoparticles were formed in situ as interfacial products via the reaction between Ti and GO during sintering. With increases in GO content and sintering temperature, the amount of TiC increased, improving the mechanical properties of the composites. GO was also partly retained with a lamellar structure after sintering. The composite reinforced with 5 wt% GO exhibited a hardness of 457 HV, 48.4% higher than that of pure Ti at 1473 K. The Ti-2.5 wt% GO composite sintered at 1473 K achieved a maximum yield stress of 1294 MPa, which was 62.7 % higher than that of pure Ti. Further increasing the GO content to 5 wt% led to a slight decrease in yield stress owing to GO agglomeration. The fracture morphology of the composite reinforced with GO exhibited a quasi-cleavage fracture, whereas that of the pure Ti matrix showed a ductile fracture. The main strengthening mechanism included grain refinement, solution strengthening, and dispersion strengthening of TiC and GO.

In this work, eco-friendly superhydrophobic coatings were prepared by dispersing hydrophobic silica nanoparticles and a waterborne silicone-modified polyurethane dispersion into an ethanol solution, which was free of fluorine and volatile toxic solvents. The effects of the silica content on the hydrophobicity and scratch resistance of the hydrophobic surfaces were investigated by WCA measurements and a sandpaper abrasion test, respectively. The experimental results indicated that when the silica content exceeded 30% by mass, the silica/silicone-modified polyurethane coatings had superhydrophobicity. Meanwhile, the superhydrophobic coatings with a silica content of 30% by mass simultaneously had the optimal mechanical stability. We studied the morphology and roughness of the hydrophobic surfaces with different silica content and attempted to briefly explain the influence mechanism of silica content. Furthermore, anti-icing and oil–water separation experiments were carried out on the superhydrophobic coatings, which exhibited good anti-icing performance and high separation efficiency. The eco-friendly superhydrophobic coating is expected to be applied in the fields of oil–water separation, anti-icing, and self-cleaning, etc.

A pulse laser combined LWT technique with a two-stage reconstruction algorithm was proposed to realize rapid damage location, or even the evaluation of damage size for plate-like structures. Since the amplitude of Lamb waves in propagation is highly sensitive to damage, including inside damage, the change of the attenuation coefficient of Lamb waves in the inspection region was used as a damage index to reconstruct damage images. In stage one, the rough area of the damage was identified by a comparison of the amplitude of the testing signal data and reference data (undamaged state). In stage two, the damage image was reconstructed using an inverse approach based on the least-square method. In order to verify the effectiveness of the proposed rapid approach, experiments on an aluminum plate with a non-penetrating notch and a carbon fiber-reinforced plastic laminated plate with internal delamination induced by a low-velocity impact were carried out. The results show that the notch can be detected with accurate location, and the delamination image can be reconstructed successfully.

This paper investigates the propagation of low-frequency S₀ mode Lamb waves in plates with quadratic nonlinearity through numerical simulations and experimental measurements. Both numerical and experimental results manifest distinct ultrasonic nonlinear behavior which is mainly presented by the second harmonics. Meanwhile, we find that both the acoustic nonlinearity parameter and dispersion distance show the exponential decay trend with the increase of frequency-thickness. Moreover, the results reveal that the frequency is key to affect the acoustic nonlinearity parameter and dispersion distance with the same frequency-thickness. This study theoretically and experimentally reveals that nonlinear Lamb waves of the low-frequency S₀ mode are feasible to quantitatively identify material weak nonlinearity in plates.