The solution heat treatment (SHT) of the third generation of single crystal (SC) Ni-based superalloys required up to 45 h and was expensive. In this study, SHT based on liquid metal cooling (LMC) was optimized to greatly reduce processing time. The experimental and simulation results showed that residual segregation was evidently reduced, e.g., from 2.12 to 1.22 for the most heavily segregated Re. This led to a 16.7% increase in creep life, more uniform microstructures, and a decrease in solidification and homogenization porosity by a factor of 3.4. Structural refinement, approximately 0.32 times, served as the underlying mechanism for this optimization, which reduced diffusion distance and increased homogenization efficiency during SHT.
The tensile and compression fatigue deformation tests of AZ31 magnesium alloy were carried out at room temperature, and the activation behavior of {10-12}-{10-12} secondary twins in different loading directions (ND normal direction, RD rolling direction) and different strain amplitude (0.5%, 1%) was studied. The results showed that {10-12}-{10-12} secondary twins were observed on the fracture surface of the fatigue samples in the ND at the strain of 1%. In contrast, no secondary twins were observed in the ND at the strain of 0.5% nor in the RD at the strain of 1% and 0.5%, and the fatigue life in the ND was greater than that in the RD. The analysis showed that the generation of {10-12}-{10-12} secondary twins was associated with the grain size and loading direction and that the fatigue deformation at 1% strain was more likely to generate {10-12}-{10-12} secondary twins due to the large lamellar thickness of the primary twins generated at relatively large strain conditions. The fatigue deformation along the ND tension was more favorable for the activation of multiple {10-12} primary twins, and the interaction of multiple twin variants was more favorable to activate {10-12}-{10-12} secondary twins.
The roles of traveling magnetic fields (TMFs) within the transport phenomena during the directional solidification of nickel-based superalloys were simulated. The evolution of thermal field, flow field and solid-liquid interface morphology during the solidification process under both natural and forced convection conditions were also simulated and compared. The strength of TMFs window that suppresses the flow of the interfacial front in the melt was quantified. The association between flow velocity at the interface front and defect formation was discussed.
10 December 2025 in Crystal Research and Technology