When using a high concentration of reclaimed asphalt pavement (RAP) in a recycled hot-mix asphalt mixture (RHMA), the degree of blending of the reclaimed asphalt binder significantly affects the performance of the RHMA. Hence, it is essential to know the degree of blending of the RAP and its effect on the performance and the environmental impact of RHMA in order to determine the optimal mixing duration. To this end, the dispersion of reclaimed asphalt was observed using artificial RAP and the image analysis method, and the blending of reclaimed asphalt in RHMA with different mixing durations was also evaluated using physical properties tests, a rheometer test, a Fourier-transform infrared spectroscopy (FTIR) test, a gel permeation chromatography (GPC) test, and an atomic force microscope (AFM) test. The performance of RHMA with the different mixing durations in the plant and in the laboratory was tested using a Marshall stability test, rutting resistance test, freeze–thaw splitting test, and low-temperature bending beam test. In addition, the environmental impact of RHMA at different mixing durations was evaluated, and the optimal mixing duration was determined. The results showed that the mixing duration had a significant influence on the dispersion and blending of reclaimed asphalt in RHMA. The longer the mixing duration was, the higher the dispersion and the degree of blending of the reclaimed asphalt in the RHMA were. With the increase in the mixing duration, the properties, chemical composition, and micromorphology of the blended asphalt binder tended to become similar to those of reclaimed asphalt. The performance of RHMA was improved with the increase in mixing duration; however, the energy consumption and CO2 emissions for the RHMA increase significantly with the increase in mixing time. The recommended optimal mixing durations in the mixing plant and in the laboratory were found to be 60 s and 90 s, respectively, considering the environmental impact, the RHMA production efficiency, and the performance of the RHMA.
China’s highway asphalt pavement has entered the stage of major repair, and improving the utilization rate of recycled asphalt pavement (RAP) is the main issue. The key link affecting the performance of recycled asphalt mixtures is the regeneration of aged asphalt, and the effect of the regenerant dosing on the high-temperature performance and viscosity of aged asphalt is the main content to be studied in this research. The aging behavior of asphalt seriously affects the roadworthiness of asphalt mixtures. In this study, we investigated the effect of changes in the microscopic properties of the aged asphalt on its viscosity properties during regeneration using gel permeation chromatography (GPC), Fourier-transform infrared spectroscopy (FTIR), and atomic force microscopy (AFM) as well as Brinell viscosity tests. This study simulated asphalt aging by the RTFOT test, and then we obtained an aged asphalt with a needle penetration of 30. We prepared different regenerated asphalts by adding regeneration agent with doses of 2%, 4%, and 6% to the aged asphalt. The results showed that the regeneration agent could effectively reduce the viscosity of the aged asphalt, which can play a positive role in improving the construction and ease of the aged asphalt. Rejuvenation agents affected the aging asphalt sulfoxide and carbon group indices. Moreover, rejuvenation agents can also significantly reduce the intensities of their characteristic functional group indices. The results of the AFM test showed that the increase in the dose of regeneration agent increased the number of the asphalt bee-like structures and decreased the area of individual bee-like structures. The results of the GPC test were consistent with the results of the AFM test, and the increase in the dose of regeneration agent reduced the asphalt macromolecule content. The viscosity properties and microstructure of the aged asphalt changed positively after the addition of the regeneration agent, indicating that the regeneration agent had a degrading and diluting effect on macromolecules.
This study focuses on the effect of oils on rheology and oxidation aging of Styrene-Butadiene-Styrene modified asphalt (SBSMA) in the long term, after reducing one low-temperature Performance Grade (PG) of SBSMA by incorporating oils. Two oils, including corn-based bio-oil and re-refined engine oil bottom (REOB), were selected to enhance the low-temperature performance of SBSMA. All samples were subjected to Rolling Thin Film Oven (RTFO) aging and 20-h as well as 40-h Pressure Aging Vessel (PAV20 and PAV40) aging, prior to multiple stress creep recovery (MSCR), frequency sweep and Flourier transform infrared spectroscopy (FTIR) scanning. A good high-temperature performance of oil/SBS modified asphalt blends was reflected in MSCR and PG results, meanwhile non-recoverable creep compliance (Jnr) and recovery (R) were found to share a highly correlated relationship during aging progress. In addition, Glover–Rowe (G–R) parameter and phase angle master curves suggest that the improvement of cracking property mainly came from the softening effect of oils. Adding oils into SBSMA was observed to increase oxidation kinetics, but the blends with oils still exhibited better anti-oxidation aging than the base binder, mainly due to the SBS addition. Bio-oil exhibited an effect of relieving age hardening susceptibility of SBSMA.
Asphalt binders that perform exceptionally well in resisting both rutting and cracking are highly desirable for withstanding the combined effects of extreme low temperatures and heavy vehicle loads. This work highlights the benefits of softening oils on the cracking performance of styrene–butadiene–styrene-modified asphalt (SBSMA). Additionally, the inherent correlations between cracking-performance parameters of binders and mixtures were thoroughly analyzed. A bio-based oil (bio-oil) and a petroleum-based oil (re-refined engine oil bottom, REOB) were selected as the softening oils. The benefit provided by softening oils was evaluated using various rheological indices, while the adverse effects of oxidative aging on cracking resistance were also considered. The cracking properties at intermediate temperatures were characterized by the modified Glover–Rowe (M G–R) parameter, δ8967 kPa, and fatigue life (Nf). The low-temperature cracking properties of binders were evaluated by stiffness and m-value. The indirect tensile asphalt cracking (IDEAL-CT) test was conducted utilizing the CT-index and post-peak slope to estimate the fracture properties of the mixtures. The oxidative aging of binder and mixture samples was simulated and carried out based on lab aging methods; meanwhile, the carbonyl index obtained from the Fourier transform infrared (FTIR) scanning was used to track and evaluate the aging level of binders. The results show that the cracking performance could be greatly improved by the application of softening oils. Meanwhile, the bio-oils were found to operate with much higher efficiency than REOB, since the oil modification index (OMI) result showed that bio-oils exhibited four to six times the efficiency of REOB, in terms of improving the stress relaxation property. The correlations proved that the cracking-related parameters shared an inherent relationship with R2 above 0.85, while these parameters consistently declined as the binder aged. The cracking performance of the mixtures at intermediate temperatures was mainly governed by the fatigue life of the binder, whereas thermal cracking performance was highly associated with the binder’s relaxation property.