The effect of compound fields of ultrasonic vibration and applied pressure (UV+AP) on three-dimensional (3D) microstructure and tensile properties of recycled Al-Cu-Mn-Fe-Si alloys was systematically studied using conventional two-dimensional (2D) microscopy, synchrotron X-ray tomography, and tensile test. The properties of UV+AP treated alloys with the pouring temperature of 740, 710 and 680 °C were compared when those alloys achieved after gravity casting. After UV+AP treatment, the alloy with pouring temperature of 710 °C show the smallest grain size. Also, the sizes of Fe-rich phases and Al2Cu are greatly reduced and their 3D morphologies are compacted. The mechanical properties of UV+AP treated alloys are relatively higher than those measured for gravity cast equivalents. This improvement can be explained by the synergistic effect of acoustic cavitation, acoustic streaming, and force-feeding, which resulted in the dendrite fragmentation, uniform solute distribution, and microstructural refinement. The Orowan strengthening and solution strengthening were identified as the main strengthening mechanisms.
1 November 2018 in Materials Science and Technology
Effects of added Al–5Ti–B master alloys on precipitation of iron-rich intermetallics and mechanical properties of A356 cast alloys with high Fe content (1.5 wt-%) were investigated using image analysis, scanning electron microscopy, and tensile testing. Results show that added Al–5Ti–B has apparent refinement on α (Al) grain size of A356 alloys that have high Fe content. 12 wt-% Al–5Ti–B is beneficial for improving mechanical properties of A356 cast alloys with high Fe content. Improved mechanical properties can be attributed to refined microstructure, the proper amounts of TiB2 and Ti(AlSi)3, and decreased porosity. An excessive amount of Al–5Ti–B deteriorates mechanical properties of alloys because it leads to the formation of large secondary intermetallics and increased porosity.
17 September 2024 in Transactions of Nonferrous Metals Society of China
Effects of ultrasonic vibration (UV) and mechanical vibration (MV) on the Mn-rich phase modification and mechanical properties of Al−12Si−4Cu−1Ni−1Mg−2Mn piston alloys were investigated. The results show that the UV and UV+MV treatments can significantly refine and fragmentize the microstructures. In addition, UV treatment can significantly passivate the primary Mn-rich Al15Mn3Si2 intermetallics. The formation mechanisms of refinement and passivation of the grains and non-dendrite particles were discussed. Compared with the gravity die-cast alloys, the UV and UV+MV treated alloys exhibit improved tensile and creep resistance at room and elevated temperatures. These results can be attributed to the refinement of the α(Al) grains and the secondary intermetallics, the increased proportion of refined heat-resistant precipitates, and the formation of nano-sized Si particles. The ultimate tensile strength of the UV treated alloys at 350 °C exceeds that of commercial piston alloys. This indicates the high application potential of the developed piston alloys in density diesel engines.
The iron-rich intermetallics are considered to be stable in aluminium alloys and usually hard to dissolve into the matrix during solution heat treatment (SHT). Nevertheless, solid-state transformations between Fe-rich intermetallics may happen and will play a great role in breaking-up of the large Fe-rich intermetallics particle during hot deformation process. In this study, the solid-state phase transformation of the iron-rich intermetallics from AlmFe to β-Fe (Al7Cu2Fe) has been studied using SEM, XRD and deep-etched technique in a 2xxx Al–Cu cast alloy during SHT. The mechanism of solid-state transformation for the Fe-rich intermetallics was discussed, including the solid-state reaction, nucleation and growth of iron-rich intermetallics and Al phases.