XANES and SR-TXM were used to investigate the fates of MoS ₂ -PVP nanosheets in vivo and in vitro .

Inorganic nanomaterials are pivotal foundational materials driving traditional industries’ transformation and emerging sectors’ evolution. However, their industrial application is hindered by the limitations of conventional synthesis methods, including poor batch stability, scaling challenges, and complex quality control requirements. This review systematically examines strategies for constructing automated synthesis systems to enhance the production efficiency of inorganic nanomaterials. Methodologies encompassing hardware architecture design, software algorithm optimization, and artificial intelligence (AI)-enabled intelligent process control are analyzed. Case studies on quantum dots and gold nanoparticles demonstrate the enhanced efficiency of closed-loop synthesis systems and their machine learning-enabled autonomous optimization of process parameters. The study highlights the critical role of automation, intelligent technologies, and human–machine collaboration in elucidating synthesis mechanisms. Current challenges in cross-scale mechanistic modeling, high-throughput experimental integration, and standardized database development are discussed. Finally, the prospects of AI-driven synthesis systems are envisioned, emphasizing their potential to accelerate novel material discovery and revolutionize nanomanufacturing paradigms within the framework of AI-plus initiatives.

Nanocomposites of Cu ₂ (OH)PO ₄ and rGO exhibit the maximized infrared light photocatalytic activity for the degradation of 2,4-DCP due to the combination of the photocatalytic and photo-Fenton effects into one reaction system.

Silica aerogels are three-dimensional porous materials that were initially produced in 1931. During the past nearly 90 years, silica aerogels have been applied extensively in many fields.

Addressing the problem of high chemical oxygen demands (COD) of cutting fluid waste generated in the machining process, its complex composition, and the specific conditions required for the treatment process, a heterogeneous Fenton fibre catalyst (NZVI@ACF) made of nanometer-iron supported on activated carbon fiber using dip-molding was developed. NZVI was homogeneously loaded onto ACF surfaces to form NZVI@ACF, with a specific surface area (S_BET) of 726.3642 m²/g. Using a multistage chemical pretreatment, the NZVI@ACF/H₂O₂ system was used to effectively treat cutting fluid waste. The results indicated that the rate of COD removal in the cutting fluid waste liquid pretreated with NZVI@ACF/H₂O₂ system was 99.8% when the reactions conditions were optimized to 20 nmol/L H₂O₂, 6 g/L NZVI@ACF, total reaction time of 120 min and pH 5. The treated waste solution passed China’s tertiary wastewater discharge standards. NZVI@ACF/H₂O₂ demonstrated an excellent catalytic performance compared to the traditional Fenton catalyst, increased the effective pH reaction range and had an adsorption effect on the waste liquid after the reaction.