The source profile of volatile organic compounds (VOCs) is essential for establishing reactivity- and toxicity-based emission inventories and developing effective air pollution control strategies. In this paper, the establishment of VOC source profiles and the VOC emission characteristics are reviewed in the petrochemical, solvent use, and chemical industries, and the most up-to-date profiles of the three industries in China are compiled via necessary adjustment and reconstruction of the test data from the literature. Alkanes dominated and OVOCs were often neglected in the overall petrochemical industry and refined processes. They accounted for 60.6% and 3.2% in the merged profiles. Aromatics and OVOCs dominated in the industrial solvent use industry. OVOCs were the most prevalent in the printing and dyeing industries, furniture manufacturing industries, and automobile coating process, whereas aromatics were major contributors of the total VOCs in metal surface coating, shipping coating, and other surface coating industries in the merged profiles. A wide range of products and limited profile studies were obtained in chemical industry, and the compositions of VOCs varied significantly in the production of 30 products in the merged profile. The future research directions of VOC source profiles are discussed, mainly focusing on the sampling, establishment, and evaluation of VOC profiles.