This study investigates the contact temperatures caused by frictional heating of sliding parallel pairs. In this case the materials studied are a PTFE composite in contact with a high carbon steel plate. These materials are commonly used for industrial applications, in particular as the main contacting components within a scroll expander system. The expected contact temperature values are important to be quantified in order to predict failure mechanisms associated with excessive thermal effects caused by sliding friction. A rational and coherent interpretation of the thermal effects on the actual tribological contact is presented.Contact temperatures are monitored continuously using a high-precision infrared thermal imaging technique with a systematic variation in surface roughness of the high carbon steel material. These surface temperatures are investigated as a function of the friction coefficient, the sliding velocity and the applied load while the most influential parameter for the temperature rise is determined. Analytical results using conventional mathematical methodology are also produced. The analytical and experimental findings are then compared indicating interesting correlations within the macro- and micro-surface temperature regimes and the experimental conditions. Microscopic observations show that thermal effects can seriously affect fibers durability while transfer films formed across the steel counterpart can be beneficial for the operation of scroll systems under specific roughness and test conditions
High temperature nanoindentation is an emerging field with significant advances in instrumentation, calibration, and experimental protocols reported in the past couple of years. Performing stable and accurate measurements at elevated temperatures holds the key for small scale testing of materials at service temperatures. We report a novel high temperature vacuum nanoindentation system, High Temperature Ultra Nanoindentation Tester (UNHT3 HTV), utilizing active surface referencing and non-contact heating capable of performing measurements up to 800 °C. This nanoindenter is based on the proven Ultra Nano-Hardness Tester (UNHT) design that uses two indentation axes: one for indentation and another for surface referencing. Differential displacement measurement between the two axes enables stable measurements to be performed over long durations. A vacuum level of 10−7 mbar prevents sample surface oxidation at elevated temperatures. The indenter, reference, and sample are heated independently using integrated infrared heaters. The instrumental design details for developing a reliable and accurate high temperature nanoindenter are described. High temperature calibration procedures to minimize thermal drift at elevated temperatures are reported. Indentation data on copper, fused silica, and a hard coating show that this new generation of instrumented indenter can achieve unparalleled stability over the entire temperature range up to 800 °C with minimum thermal drift rates of <2 nm/min at elevated temperatures.
1 September 2014 in The Journal of Physical Chemistry C