In the present study, composites incorporating NiO-Co₃O₄ (NC) and CuO-NiO-Co₃O₄ (CNC) as active electrode materials were produced through the hydrothermal method and their performance was investigated systematically. The composition, formation, and nanocomposite structure of the fabricated material were characterized by XRD, FTIR, and UV–Vis. The FE-SEM analysis revealed the presence of rod and spherical mixed morphologies. The prepared NC and CNC samples were utilized as supercapacitor electrodes, demonstrating specific capacitances of 262 Fg⁻¹ at a current density of 1 Ag⁻¹. Interestingly, the CNC composite displayed a notable long-term cyclic stability 84.9%, which was observed even after 5000 charge–discharge cycles. The exceptional electrochemical properties observed can be accredited to the harmonious effects of copper oxide addition, the hollow structure, and various metal oxides. This approach holds promise for the development of supercapacitor electrodes. These findings collectively indicate that the hydrothermally synthesized NC and CNC nanocomposites exhibit potential as high-performance electrodes for supercapacitor applications.

In this study, novel V₂O₅-decorated garlic peel biochar (VO/GPB) nanocomposites are prepared via the facile hydrothermal technique. As-synthesized VO/GPB is characterized by various spectroscopic and analytical techniques. The surface morphology of the as-prepared samples was predicted by SEM analysis, which shows that the block-like V₂O₅ was uniformly decorated on the stone-like GPB surface. The elemental mapping analysis confirms the VO/GPB composite is composed of the following elements: C, O, Na, Mg, Si, P, K, and V, without any other impurities. The photocatalytic activity of the VO/GPB nanocomposite was examined by the degradation of methyl orange (MO) under the irradiation of visible light; 84% degradation efficiency was achieved within 30 min. The reactive oxidative species (ROS) study reveals that hydroxyl and superoxide radicals play an essential role in MO degradation. Moreover, the antioxidant action of the VO/GPB nanocomposite was also investigated. From the results, the VO/GPB composite has higher antioxidant activity compared to ascorbic acid; the scavenging effect increased with increasing concentrations of VO/GPB composite until it reached 40 mg/L, where the scavenging effect was the highest at 93.86%. This study will afford innovative insights into other photocatalytic nanomaterials with effective applications in the field of photocatalytic studies with environmental compensation.