The aim of the work is to study the effect of the 3D printing process on the microstructural and hydrophilic properties of polylactic acid (PLA) samples with various model printing patterns obtained from the black filament PLA by sequentially applying polymer layers using the FDM (fused deposition modeling) method. X-ray phase analysis revealed the partial crystallization of PLA polymer chains in the printed samples, which occurs under thermal and mechanical action on the original amorphous PLA filament during 3D printing to varying degrees, depending on the geometry of the pattern and the morphology of its surface. At the same time, IR spectroscopy data indicate the preservation of all intrastructural chemical bonds of polylactide. Measured at the original installation, the values of the wetting edge angles on the surface of the printed samples are in the range φ = 50–60°, which is significantly less than the right angle. This indicates the hydrophilic properties of the whole sample’s surface. At the same time, the influence of different geometries of model drawings in printed samples was found not only on the morphology of the sample’s surface according to SEM data but also on its wettability.

The aim of the work is to study the effect of the 3D printing process on the microstructural and hydrophilic properties of polylactic acid (PLA) samples with various model printing patterns obtained from the black Filament PLA by sequentially applying polymer layers using the FDM (Fused Deposition Modeling) method. X-ray phase analysis revealed partial crystallization of PLA polymer chains in printed samples, which occurs under thermal and mechanical action on the original amorphous PLA filament during 3D printing to varying degrees, depending on the geometry of the pattern and the morphology of its surface. At the same time, IR spectroscopy data indicate the preservation of all intrastructural chemical bonds of polylactide. Measured at the original installation, the values of the wetting edge angles on the surface of the printed samples are in the range φ = 50-60°, which is significantly less than the right angle. This indicates the hydrophilic properties of all samples’ surface. At the same time, the influence of different geometries of model drawings in printed samples was found not only on the morphology of the samples’ surface according to SEM data, but also on its wettability.

В работе исследованы фазовый состав и его изменения при температурных отжигах порошкового сплава Co₆₆Cr₂₈Mo₆ и зубной коронки, полученной из того же порошка с помощью 3D- печати методом селективного лазерного плавления. Рентгенодифракционные исследования исходного порошка Co₆₆Cr₂₈Mo₆ и неотожженной коронки показали, что лазерная печать полностью переводит двухфазный порошок (90 % ГЦК +10 % ГПУ) в однофазный твердый раствор ГЦК на основе высокотемпературной гранецентрированной кубической модификации b-Со с заметным увеличением межплоскостных расстояний по сравнению с b-Со.   Работа выполнена при поддержке Минобрнауки России в рамках государственного задания ВУЗам в сфере научной деятельности на 2017-2019 годы. Проекты № 3.6263.2017/ВУ и № 16.8158.2017/8.9.