BACKGROUND—The solid-phase joining of A6082-T6 plates by bobbin friction stir welding (BFSW) is problematic. Better methods are needed to evaluate the microstructural evolution of the weld. However, conventional Al reagents (e.g., Keller’s and Kroll’s) do not elucidate the microstructure satisfactorily, specifically regarding grain size and morphology within the weld region. APPROACH—We developed innovative etchants for metallographic observations for optical microscopy. RESULTS—The macrostructure and microstructure of A6082-T6 BFSW welds were clearly demonstrated by optical microscopy analysis. The microetching results demonstrated different microstructures of the Stir Zone (S.Z) distinct from the Base Metal (B.M) and Heat Affected Zone (HAZ) & Thermo-mechanical Affected Zone (TMAZ). The micrographs showed a significant decrease in grain size from 100 μm in B.M to ultrafine 4–10 μm grains for the S.Z. Also, the grain morphology changed from directional columnar in the B.M to equiaxed in the S.Z. Furthermore, thermomechanical recrystallization was observed by the morphological flow of the grain distortion in HAZ and TMAZ. The etchants also clearly show the polycrystalline structure, microflow patterns, and the incoherent interface around inclusion defects. ORIGINALITY—Chemical compositions are identified for a suite of etchant reagents for metallographic examination of the friction-stir welded A6082-T6 alloy. The reagents have made it possible to reveal microstructures not previously evident with optical microscopy.

Bobbin friction stir welding (BFSW), with its fully penetrated pin and double-sided shoulder, can provide high rates of heat generation. This produces solid-state thermo-mechanical grain refinement. In this paper, the microstructure evolution of the welded joints of AA6082-T6 obtained using BFSW process was investigated with a focus on grain refinement. Two sheets of the AA6082-T6 alloy were butt-welded with a fixed-gap bobbin tool. The microstructure at a mid-weld transverse cross-section was evaluated using optical microscopy and electron backscatter diffraction (EBSD). Significant grain refinement was observed, with a decrease in grain size from 100 μm in directional columnar grain morphology of the base metal, to an ultrafine size—less than 10 μm—for the equiaxed grains in the stirring zone. The EBSD results showed that with BFSW processing, secondary phase precipitation patterns were produced that are distinct from the primary artificial age-hardening precipitates created by the T6 tempering cycle. The severe plastic deformation and heat generation appear to accelerate dynamic recrystallization and precipitation during the BFSW process. The microstructural studies confirmed that the BFSW process can provide a highly efficient thermodynamically activated grain refinement in the solid-state without requiring additional processes such as heat treatment or external means of grain refinement.

Bobbin friction stir welding (BFSW) is an innovative variant for the solid state welding process whereby a rotating symmetrical tool causes a fully penetrated bond. Despite the process development, there are still unknown variables in the characterization of the process parameters which can cause uncontrolled weld defects. The entry zone and the exit zone consist of two discontinuity-defects and removing them is one of the current challenges for improving the weld quality. In the present research, the characteristic features of the entry and exit defects in the weld structure and formation mechanism of them during the BFSW processing was investigated. Using stacked layers of multi-colour plasticine the material flow, analogous to metal flow, can be visualised. By using different colours as the path markers of the analogue model, the streamline flow can be easily delineated in the discontinuity defects compared with the metal welds. AA6082-T6 aluminium plates and multi-layered plasticine slabs were employed to replicate the entry-exit defects in the metal weld and analogue samples. The fixed-bobbin tool utilized for this research was optimized by adding a thread feature and tri-flat geometry to the pin and closed-end spiral scrolls on both shoulder surfaces. Samples were processed at different rotating and longitudinal speeds to show the degree of dependency on the welding parameters for the defects. The analogue models showed that the entry zone and the exit zone of the BFSW are affected by the inhomogeneity of the material flow regime which causes the ejection or disruption of the plastic flow in the gap between the bobbin shoulders. The trial aluminium welds showed that the elimination of entry-exit defects in the weld body is not completely possible but the size of the defects can be minimized by modification of the welding parameters. For the entry zone, the flow pattern evolution suggested formation mechanisms for a sprayed tail, island zone and discontinuity-channel. For the exit zone a keyhole-shaped discontinuity is discussed as a structural defect.

The effect of various tungsten carbide (WC) pin tools and operating parameters on the material structure and properties of an AA1100 friction stir welding (FSW) weld were evaluated. Three different pin shapes were employed (conical, square and threaded). For each tool shape, welds were generated for a set of tool (revolutions per minute, RPM) (710, 1120 and 1400) and advancing speeds (150, 250 and 400 mm/min). Weld samples were tested for mechanical strength by tensile testing. Morphology was examined using optical microscopy, and weld composition with scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS) and X-ray diffraction (XRD). No weld contamination from the tools was observed. However, a number of structural defects, inherent to the FSW process, were observed (including tunnel voids, kissing bonds and swirling lines). These defects, associated with the stirring action, could not be eliminated. The results show how the operating parameters may be optimized to produce stronger welds.

Material flow transportation around the rotating tool and the mass deposition at the backside of the tool are critical characteristics of friction stir welding. To achieve an optimized weld structure, the history of the plastic deformation needs to be identified with a flow-based elucidation. In this study, an analogue model was applied to evaluate the formation of a banded structure using the bobbin tool, with a focus on the interaction between the tool-workpiece. The flow visualization in plasticine analogue was validated in comparison with the aluminium welds. The plastic flow mechanism was visualized both, at the surface and the cross-section of the weld-seam. The cross-section of the weld shows the details of the formation of tunnel voids, caused by the failure of the flow regimes. A physical model of the material flow was proposed to explain the formation mechanism of the tunnel void as a discontinuity during the mass refilling at the rear of the tool.

One of the difficulties with bobbin friction stir welding (BFSW) has been the visualisation of microstructure, particularly grain boundaries, and this is especially problematic for materials with fine grain structure, such as AA6082-T6 aluminium as here. Welds of this material were examined using optical microscopy (OM) and electron backscatter diffraction (EBSD). Results show that the grain structures that form depend on a complex set of factors. The motion of the pin and shoulder features transports material around the weld, which induces shear. The shear deformation around the pin is non-uniform with a thermal and strain gradient across the weld, and hence the dynamic recrystallisation (DRX) processes are also variable, giving a range of observed polycrystalline and grain boundary structures. Partial DRX was observed at both hourglass boundaries, and full DRX at mid-stirring zone. The grain boundary mapping showed the formation of low-angle grain boundaries (LAGBs) at regions of high shear as a consequence of thermomechanical nature of the process.