Based on the excellent comprehensive mechanical properties of high–entropy alloy (HEA), the NiAl-based HEA was designed to achieve excellent high-temperature strength, toughness, and wear resistance. In this work, vacuum arc melting technology was used to prepare (NiA1)₇₈(CoCrFe)_16.5Cu_5.5 HEA, and its microstructure, phase composition, and mechanical properties were systematically studied. The results showed that (NiA1)₇₈(CoCrFe)_16.5Cu_5.5 HEA was composed of FCC and BCC/B2, with a spinodal decomposition structure in the matrix, and nano-precipitation in the interdendritic, exhibiting a good high-temperature performance. At 600 °C, the compressive fracture strength is 842.5 MPa and the fracture strain is 24.5%. When the temperature reaches 800 °C, even if the strain reaches 50%, the alloy will not fracture, and the stress–strain curve shows typical work hardening and softening characteristics. The wear coefficient of the alloy first increases and then decreases with the increase in temperature in the range of room temperature to 400 °C. However, the specific wear rate shows the opposite trend. At 100 °C, the wear rate reaches the lowest of 7.05 × 10⁻⁵ mm³/Nm, and the wear mechanism is mainly abrasive wear.

Al-Si-Mg alloy has excellent casting performance due to its high silicon content, but the coarse eutectic silicon phase can lead to a decrease in its mechanical properties. Samples of AlSi10Mg alloy were prepared by using a spark plasma sintering method, and it was found that sintering temperature has a significant impact on the grain size, eutectic silicon size and wear and corrosion properties after heat treatment. At a sintering temperature of 525 °C, the alloy exhibits the best wear performance with an average friction coefficient of 0.29. This is attributed to the uniform precipitation of fine eutectic silicon phases, significantly improving wear resistance and establishing adhesive wear as the wear mechanism of AlSi10Mg alloy at room temperature. The electrochemical performance of AlSi10Mg sintered at 500 °C is the best, with I_corr and E_corr being 1.33 × 10⁻⁶ A·cm⁻² and −0.57 V, respectively. This is attributed to the refinement of grain size and eutectic silicon size, as well as the appropriate Si volume fraction. Therefore, optimizing the sintering temperature can effectively improve the performance of AlSi10Mg alloy.

The effects of Si, Fe and Zr elements on the high temperature properties and microstructure of ultrathin 3003mod aluminum alloy fins were studied by means of high-temperature tensile tests, sagging tests and microstructure analyses. The results show that the alloying of Si, Fe, and Zr elements formed a large amount of nano-scale α-Al(Mn,Fe) Si and Al₃Zr particles, and significantly reduced the number of micro-scale coarse Al₆(Mn,Fe) particles in the 3003mod aluminum alloy, exhibiting 5 to 10 MPa higher strength and better sagging resistance than 3003 aluminum alloy at the same temperature. The variations in properties such as high-temperature mechanical properties, sagging resistance and elongation below 400 °C were ascribed to the high-stability nanoparticles effectively preventing recovery and grain boundary migration, as well as reducing the nucleation cores of recrystallization. The nanoparticles in 3003mod aluminum alloy were coarsened significantly at 500 °C, and the grains were completely recrystallized and coarsened, resulted in a significant decrease in strength, sagging resistance and elongation compared with these at 400 °C.