Bending fatigue significantly affects the mechanical stability and lifespan of biomedical implants, such as bone plates and orthopaedic fixation devices, which undergo cyclic loading in the human body. This study examines the microstructure, porosity, and bending fatigue properties of PBF-LB/M SS316L. Samples were analysed across three faces (top, front, and side) using optical microscopy (OM) and scanning electron microscopy (SEM) to observe microstructural features and porosity. Elemental composition was measured by energy-dispersive X-ray spectroscopy (EDX). Phase structures and grain orientations were characterised via X-ray diffraction (XRD) and electron backscatter diffraction (EBSD). Four-point bending fatigue tests, conducted under two loading conditions, below and slightly above the yield point, demonstrated that defects inherent to the PBF-LB/M process, particularly micropores and unmelted powder particles, strongly influence fatigue crack initiation. Real-time monitoring of crack initiation and propagation on the external sample surface was performed using a high-speed digital microscope. These findings indicate the influence of microstructural defects on fatigue performance in PBF-LB/M SS316L, supporting the design and development of more reliable patient-specific biomedical implants.
In this study, an appropriate scanning strategy in selective laser melting [SLM, also known as laser powder bed fusion (LPBF)] was adopted to enhance the forming quality of stainless steel (SS) 316L for load-bearing implant applications, with a particular focus given to investigate the effect of argon flow velocity inside the build chamber. The biocompatibility of the resulting printed surfaces was evaluated by in vitro culturing of mesenchymal stem cells (MSCs) at different time points up to 96 h. Notably, it is one of the first studies to document the MSC response on SLM 316L surfaces. The results showed that highly dense parts (>99.8% density) can be produced by carefully selecting the interlayer rotation, scan vector length, and hatch distance. Microsized surface defects (i.e., balling) appeared after the SLM process. Their chance of occurrence and size were found to be related to the gas flow velocity inside the build chamber. The resulting printed surfaces were hospitable for MSCs, and healthy cell response was recorded throughout the 96-h culture periods. These findings can be instrumental in optimizing the surface features of SLM in order to improve the cell response.
This study investigated the effects of Zinc (Zn) content, specifically in the range of 1 wt.% to 7 wt.%, on the powder characteristics, porosity, microstructure, and corrosion behavior of Mg-xZn-0.2Mn alloys produced using selective laser melting (SLM). To evaluate the porosity of the printed parts and various powder attributes, such as size, circularity, void spaces between powders, and inherent imperfections, scanning electron microscopy (SEM) and optical microscopy (OM) were employed. The alloy microstructure, composition, and phase were examined using energy dispersive X-ray (SEM-EDX) and X-ray Diffraction (XRD). The corrosion resistance and degradation behavior were assessed through electrochemical corrosion tests and immersion tests in Hanks’ solution at 37.5 °C, respectively. Finally, OM and SEM-EDX were used to characterize the corrosion products. The findings of this study indicated that the powder size increased with Zn content, maintaining a 0.8 circularity. Powder defects were minimal, with occasional satellite particles. For the SLM-printed samples, it was evident that porosity characteristics could be influenced by Zn content. As Zn content increased, the pore fraction rose from 1.0% to 5.3%, and the pore size grew from 2.2 μm to 3.0 μm. All printed samples consisted of an α-Mg matrix. Additionally, a higher Zn content resulted in more distinct grain boundaries. Corrosion resistance decreased with Zn, leading to more pronounced localized corrosion after immersion in Hanks’ solution. Ca-P was found as white corrosion products on all samples.