Accelerator mass spectrometry (AMS) is a worldwide recognized method for radiocarbon (¹⁴C) dating. The advantageous aspects of this method include the variety of materials and the small sample size (1 mg of carbon) that can be measured. However, these pose several challenges in the laboratory, such as developing appropriate chemical pretreatment methods. In the summer of 2022, the Radiocarbon and Mass Spectrometry Laboratory in Gliwice, Poland, launched the MICADAS accelerator spectrometer. The report on background and reference materials measurement results for the period from September 2022 to July 2024 is presented in this publication. Quality assurance and quality control processes are extremely important to guarantee the high quality of the results obtained in the laboratory. Hence, our Radiocarbon and Mass Spectrometry Laboratory in Gliwice took part in the Glasgow International Radiocarbon Inter-Comparison (GIRI) program. The radiocarbon ages for wood, bone, humic acid, and barley mash samples were determined and compared with reported values. The resulting data confirmed that our Laboratory is capable of dating samples across a spectrum of materials and ages ranging from contemporary to the limits of the radiocarbon method, achieving precision on par with that of other laboratories.

This paper compares various wood pretreatment methods for highly degraded, and problematic fossil wood extracted from the opencast Szczerców site of the Bełchatów Lignite Mine in Central Poland. The study evaluates the pretreatment methods using both large samples (55–255 g, referred to as series A) and small samples (36–150 mg, referred to as series B). Additionally, all preparation methods were applied to medium-sized samples (approximately 3 g, referred to as series C) with solvent washes in the Soxhlet apparatus. Radiocarbon dating was conducted using the LSC technique (subseries A₁) and the AMS technique (subseries A₂, series B, and C). The effectiveness and utility of each pretreatment protocol were compared based on ¹⁴C measurements and FTIR analysis. Through the conducted research and a multi-criteria analysis, the most effective method for preparing old fossil wood was identified. Our experience indicates that an extended, multistage preparation of highly degraded fossil wood samples, with a ¹⁴C concentration near the detection limit of the radiocarbon method, may result in a significant increase in ¹⁴C content.

Radiocarbon dating is a widely used method in archaeology and earth sciences, but the precision of calibrated dates from single radiocarbon measurements can be difficult to understand. This study investigates the precision of calibrated radiocarbon dates depending on the uncertainties of the measurement and the details of the calibration curve. Using data for the Holocene epoch and the IntCal20 calibration curve, over 1,000,000 hypothetical radiocarbon measurements were calibrated and analyzed. The study shows that high-precision measurements can yield calibrated date ranges from less than 50 years to more than 200 years (at the 95.4% probability) depending on the specifics of the calibration curve. This research may serve as a tool for planning future studies and assessing whether high-precision measurements are beneficial for proposed case.

This research paper introduces a methodology for estimating overcounting resulting from uranium series radionuclides, with a specific focus on 222Rn contamination. The method is demonstrated using the Quantulus 1220TM spectrometer. Exponential fitting is employed for the calculations, utilizing a custom algorithm developed in MATLAB® R2022b. The proposed method allows for the determination of the sample count rate correction, F14C and radiocarbon age without the need for additional chemical treatment or specialized electronics during liquid scintillation counting (LSC) measurements with the Quantulus 1220TM spectrometer. However, the method does have certain limitations. It requires a significant number of cycles and extended measurement time per cycle, but it can be applied to samples with significant 222Rn contamination that require rapid 14C analysis.

Absolute radiocarbon dating offers high precision, but its application to historical contexts, such as the Inca civilization, requires a rigorous methodological approach. This research examines methods to enhance chronological accuracy through a case study of artifacts from the Llullaillaco Capacocha sacrifice. Focusing on short‐lived organic remains, it combines radiocarbon and stable isotope analyses (carbon, nitrogen, and oxygen) to produce accurate age estimates aligned with ritual activity. To overcome hemispheric calibration issues, the study uses simulation and chronological modeling to refine temporal frameworks. This strategy advances our understanding of Inca ritual timing and broader cultural developments beyond colonial accounts by highlighting the late performance of the capacocha ritual in the context of the Inca Empire.

μGraphiline is an innovative, fully automated graphitization system designed for radiocarbon dating using accelerator mass spectrometry. This system streamlines the conversion of samples into CO2 and subsequently into graphite. The standard configuration of μGraphiline is capable of preparing 24 targets daily, demonstrating its high throughput. It achieves a graphitization efficiency of over 95% for 1 mg graphite targets. μGraphiline also offers additional modules for stepped combustion, ramped pyrolysis, and oxidation, all of which can be operated at user-defined temperatures. Furthermore, its design ensures a low background and reproducibility, significantly enhancing the accuracy and reliability of radiocarbon measurements. One of the notable advantages of the system is its low maintenance requirements. It operates efficiently without the need for working gasses such as helium (He), argon (Ar), oxygen (O2), explosive hydrogen (H2) or liquid nitrogen, which simplifies its operation and enhances safety. This feature, coupled with its modular design and high efficiency, virtually no cross-contamination between modules and samples makes μGraphiline an advanced solution for radiocarbon dating. Lastly, the system's repeatability and reliability are backed by reference materials measurements from the International Atomic Energy Agency, demonstrating good repeatability. This demonstrates μGraphiline's capability to deliver fast, consistent and accurate results, making it a valuable tool for various scientific and research applications.