Hybrids of semiconductor nanomaterials often demonstrate properties that are superior to those of their components. In this study, we prepared hybrid nanomaterials of TiO₂ and ZnO, which are among the most actively studied semiconductors, by means of millisecond-pulsed laser and analyzed how their morphology, particle size, and surface composition depend on preparation conditions. A series of nanomaterials were obtained via sequentially ablating Zn and Ti metal plates (in different sequences) in water, while laser pulses of lower (2.0 J/pulse) and higher (5.0 J/pulse) energy were applied. The properties of laser-produced hybrid TiO₂-ZnO nanomaterials were shown to be governed by experimental conditions such as laser pulse width, pulse peak power, and reaction media (either pure water or colloid with nanoparticles). The morphology revealed nanospheres of TiO₂ that decorate nanorods of ZnO or flower-like aggregates of zinc oxide. Intriguingly, after extended ablation time, titania was found to be self-doped with Ti³⁺ and Ti²⁺ ions, and the contribution of lower oxidation states of titanium could be controlled by the applied laser pulse energy. The physicochemical characteristics of hybrid nanomaterials were compared with pure ZnO and TiO₂ prepared under the same laser conditions.

Despite the known beneficial effects of creatine in treating exercise-induced muscle damage (EIMD), its effectiveness remains unclear. This study investigates the recovery effect of creatine monohydrate (CrM) on EIMD. Twenty healthy men (21–36 years) were subjected to stratified, randomized, double-blind assignments. The creatine (CRE) and placebo (PLA) groups ingested creatine and crystalline cellulose, respectively, for 28 days. They subsequently performed dumbbell exercises while emphasizing eccentric contraction of the elbow flexors. The EIMD was evaluated before and after exercise. The range of motion was significantly higher in the CRE group than in the PLA group 24 h (h) post exercise. A similar difference was detected in maximum voluntary contraction at 0, 48, 96, and 168 h post exercise (p = 0.017–0.047). The upper arm circumference was significantly lower in the CRE group than in the PLA group at 48, 72, 96, and 168 h post exercise (p = 0.002–0.030). Similar variation was observed in the shear modulus of the biceps brachii muscle at 96 and 168 h post exercise (p = 0.003–0.021) and in muscle fatigue at 0 and 168 h post exercise (p = 0.012–0.032). These findings demonstrate CrM-mediated accelerated recovery from EIMD, suggesting that CrM is an effective supplement for EIMD recovery.

This study aimed to investigate the relationship between the muscle shear modulus of the biceps brachii, urinary titin N-terminal fragment (UTF), and other damage markers after eccentric exercise. Seventeen healthy males performed five sets of ten eccentric exercises with dumbbells weighing 50% of the maximum voluntary contraction (MVC) at the elbow joint. Muscle shear modulus with range of interest set to only biceps brachii muscle measured by ultrasound shear wave elastography, UTF, MVC, range of motion (ROM), and soreness (SOR) were recorded before, immediately after, and 1, 24, 48, 72, 96, and 168 h after eccentric exercise. Each marker changed in a time course pattern, as found in previous studies. The peak shear modulus showed a moderate negative correlation with peak MVC (r = –0.531, P < 0.05) and a strong positive correlation with peak UTF (r = 0.707, P < 0.01). Our study results revealed a significant relationship between muscle strength, shear modulus measured by ultrasound SWE, and titin measured by UTF, as a non-invasive damage marker after eccentric exercise to track changes in EIMD.

We investigated the influence of advance lunging in fencing from the perspective of velocity and lower limb joint angles to identify how the joint angles contribute to the peak velocity in a lunge with advance (LWA). Fourteen skilled athletes (age: 19.6 ± 0.9 years, height: 171.2 cm ± 5.2 cm, weight: 63.7 kg ± 5.3 kg, and fencing experience: 9.7 ± 3.1 years) participated by performing two types of attacking movements, and data were collected with a 3D movement analysis system. A correlation between the peak velocity of the body center of mass (CoM) in an advance lunge and several joint angle variables (rear hip peak flexion angle (r = 0.63), rear ankle peak dorsiflexion angle (r = −0.66), rear ankle range of motion (r = −0.59), and front hip peak extension angle (r = 0.54)) was revealed. In addition, the joint angle variables that significantly predicted peak CoM velocity during an LWA were the rear knee peak flexion angle (β = 0.542), rear knee peak extension angle (β = −0.537), and front knee peak extension angle (β = −0.460). Our findings suggest that the rear leg hip joint, rear leg ankle joint, and front leg hip joint may control the acceleration generated by an LWA. Furthermore, more flexion of the rear leg knee joint in the early phase of the lunge and greater extension of the rear and front leg knee joints at the end of the lunge phase may help increase peak velocity.

Background: A recently developed smartphone application (Nordic Angle) allows the automatic calculation of the break-point angle (BPA) during Nordic hamstring exercise (NHE) without transferring the collected data to a computer. The BPA is the point at which the hamstrings are unable to withstand force. However, the validity of the BPA values obtained by this method has not been examined. Hypothesis/Purpose: This study aimed to evaluate the validity and reliability of the Nordic Angle by comparing the BPA values of the Nordic Angle with those of two-dimensional motion analysis software that can calculate the angles and angular velocities of various joints. Study Design: Cohort assessing Validity and Reliability Methods: The validity of the Nordic Angle BPA data was verified by Spearman’s correlation test for consistency with the movement analysis data, and the magnitude of the correlation was indicated by rs. The agreement between these measurements was examined using the Bland-Altman analysis. The reliability of the Nordic Angle and motion analysis was examined using the intraclass correlation coefficient (ICC) (1,k) based on data from repeated trials within a day. Results: Although the spearman correlation between the Nordic angle and the angle determined using motion analysis did not reach statistical significance (p = 0.052), a very large correlation was present (rs = 0.75). The difference between the mean values of the Nordic Angle and motion analysis was 0.4 ± 2.1°, and the limits of agreement ranged from -3.9° to 4.6°. In two BPA measurements, the Nordic Angle showed perfect reliability (ICC = 1.00, p < 0.001), while motion analysis showed nearly perfect reliability (ICC = 0.97, p < 0.001). Conclusion: The Nordic Angle, which has both validity and reliability, may be appropriate for field measurement because it allows immediate feedback of BPA and the measurement of many athletes. Level of evidence: 3b