The Portevin–Le Châtelier (PLC) effect often results in serrated plastic flow during tensile testing of aluminum alloys. Its magnitude and characteristics are often sensitive to a material’s heat treatment condition and to the applied strain rate and deformation temperature. In this study, we analyze the plastic deformation behavior of an age-hardenable Al-Cu alloy (AA2017) and of a particle reinforced AA2017 alloy (10 vol. % SiC) in two different conditions: solid solution annealed (W) and naturally aged (T4). For the W-condition of both materials, pronounced serrated flow is observed, while both T4-conditions do not show distinct serrations. It is also found that a reduction of the testing temperature (−60 °C, −196 °C) shifts the onset of serrations to larger plastic strains and additionally reduces their amplitude. Furthermore, compressive jump tests (with alternating strain rates) at room temperature confirm a negative strain rate sensitivity for the W-condition. The occurring PLC effect, as well as the propagation of the corresponding PLC bands in the W-condition, is finally characterized by digital image correlation (DIC) and by acoustic emission measurements during tensile testing. The formation of PLC bands in the reinforced material is accompanied by distinct stress drops as well as by perceptible acoustic emission, and the experimental results clearly show that only type A PLC bands occur during testing at room temperature (RT).

The precipitation kinetics of Al-Cu alloys have recently been revisited in various studies, considering either the effect of severe plastic deformation (e.g., by equal-channel angular pressing – ECAP), or the effect of particle reinforcements. However, it is not clear how these effects interact when ECAP is performed on particle-reinforced alloys. In this study, we analyze how a combination of particle reinforcement and ECAP affects precipitation kinetics. After solution annealing, an AA2017 alloy (initial state: base material without particle reinforcement); AA2017 + 10 vol.-% Al2O3; and AA2017 + 10 vol.-% SiC were deformed in one pass in a 120° ECAP tool at a temperature of 140°C. Systematic differential scanning calorimetry (DSC) measurements of each condition were carried out. TEM specimens were prepared out of samples from additional DSC measurements, where the samples were immediately quenched in liquid nitrogen after reaching carefully selected temperatures. TEM analysis was performed to characterize the morphology of the different types of precipitates, and to directly relate microstructural information to the endo- and exothermic peaks in our DSC data. Our results show that both ECAP and particle reinforcement are associated with a shift of exothermic precipitation peaks towards lower temperatures. This effect is even more pronounced when ECAP and particle reinforcement are combined. The DSC data agrees well with our TEM observations of nucleation and morphology of different precipitates, indicating that DSC measurements are an appropriate tool for the analysis of how severe plastic deformation and particle reinforcement affect precipitation kinetics in Al-Cu alloys.

In this contribution, we study the microstructural evolution of an age-hardenable AA6082 aluminum alloy during severe plastic deformation by gradation extrusion. A novel die design allowing an interruption of processing and nondestructive billet removal was developed. A systematic study on the microstructure gradient at different points of a single billet could be performed with the help of this die. Distinct gradients were investigated using microhardness measurements and electron microscopy. Our results highlight that gradation extrusion is a powerful method to produce graded materials with partially ultrafine-grained microstructures. From the point of view of obtaining an ultrafine-grained surface layer with maximum hardness, only a small number of forming elements is needed. It was also found that large incremental deformation by too many forming elements may result in locally heterogeneous microstructures and failure near the billet surface caused by localization of deformation. Furthermore, considering economical aspects of processing, fewer forming elements are preferred since several processing parameter-related cost factors are then significantly lower.

An experimental analysis of the effect of in-plane strain path changes and Bauschinger effects during mechanical loading that involves compression is quite challenging for sheet materials because they are prone to buckling. In this paper, we present a newly developed method that allows to deform sheet metals in tension and in compression. Our experimental setup primarily consists of an anti-buckling clamping device that can be used in a universal mechanical testing machine. Surface strains are measured with a digital image correlation (DIC) system. To demonstrate the viability of our method, first tests are conducted on thin sheet specimens (1 mm thickness) of a DC06 steel. Several approaches to reduce friction between the clamping system and the specimen are investigated. The validity of the test results is established in monotonic tensile tests. Measurements with different amounts of maximum tensile strain and reversed strain values are also discussed, showing that the material exhibits a Bauschinger effect, which is further quantified using different Bauschinger parameters.