The detailed examination of electron scattering in solids is of crucial importance for the theory of solid-state physics, as well as for the development and diagnostics of novel materials, particularly those for micro- and nanoelectronics. Among others, an important parameter of electron scattering is the inelastic mean free path (IMFP) of electrons both in bulk materials and in thin films, including 2D crystals. The amount of IMFP data available is still not sufficient, especially for very slow electrons and for 2D crystals. This situation motivated the present study, which summarizes pilot experiments for graphene on a new device intended to acquire electron energy-loss spectra (EELS) for low landing energies. Thanks to its unique properties, such as electrical conductivity and transparency, graphene is an ideal candidate for study at very low energies in the transmission mode of an electron microscope. The EELS are acquired by means of the very low-energy electron microspectroscopy of 2D crystals, using a dedicated ultra-high vacuum scanning low-energy electron microscope equipped with a time-of-flight (ToF) velocity analyzer. In order to verify our pilot results, we also simulate the EELS by means of density functional theory (DFT) and the many-body perturbation theory. Additional DFT calculations, providing both the total density of states and the band structure, illustrate the graphene loss features. We utilize the experimental EELS data to derive IMFP values using the so-called log-ratio method.
We explicitly derive a vortex inspired solution for the metric perturbation within the linearized Einstein general theory of relativity in arbitrary dimensions . We focus on where our solution is the gravitational analog of the well-known electromagnetic (or electron) Bessel vortex beams. Next we visualize the perturbed spacetime via tidal tendexes and frame-drag vortexes. We display and analyze mostly two-dimensional sections of the tendexes and the vortexes for different values of an angular momentum of the wave solution. Corresponding geodesic deviation equations are solved and the results are visualized. We show that the physically most important quadrupolelike case leads to a wave with rotating polarization. We discuss asymptotical features of the found solution. We provide also several 3D plots of tendex lines. One of them concerns a special cylindrical-like case and we utilize the topological classification of singularities of the depicted line fields as an approach to characterize the radiation field.
The success of machine learning (ML) models in object or pattern recognition naturally leads to ML being employed in the classification of the microstructure of steel surfaces. Light optical microscopy (LOM) is the traditional imaging process in this field. However, the increasing use of ML to extract or relate more aspects of the aforementioned materials and the limitations of LOM motivated us to provide an improvement to the established image acquisition process. In essence, we perform style transfer from LOM to scanning electron microscopy (SEM) combined with “intelligent” upscaling. This is achieved by employing an ML model trained on a multimodal dataset to generate an SEM-like image from the corresponding LOM image. This transformation, in our opinion, which is corroborated by a detailed analysis of the source, target and prediction, successfully pushes the limits of LOM in the case of steel surfaces. The expected consequence is the improvement of the precise characterization of advanced multiphase steels’ structure based on these transformed LOM images.
13 February 2022 in Surface and Interface Analysis
The segmented semiconductor detectors for transmitted electrons in ultrahigh resolution scanning electron microscopes allow observing samples in various imaging modes. Typically, two standard modes of objective lens, with and without a magnetic field, differ by their resolution. If the beam deceleration mode is selected, then an electrostatic field around the sample is added. The trajectories of transmitted electrons are influenced by the fields below the sample. The goal of this paper is a quantification of measured images and theoretical study of the capability of the detector to collect signal electrons by its individual segments. Comparison of measured and ray-traced simulated data were difficult in the past. This motivated us to present a new method that enables better comparison of the two datasets at the cost of additional measurements, so-called calibration curves. Furthermore, we also analyze the measurements acquired using 2D pixel array detector (PAD) that provide a more detailed angular profile. We demonstrate that the radial profiles of STEM and/or 2D-PAD data are sensitive to material composition. Moreover, scattering processes are affected by thickness of the sample as well. Hence, comparing the two experimental and simulation data can help to estimate composition or the thickness of the sample.