Nanoparticles are emerging as a fascinating alternative to antibiotics. When stabilized by chemical compounds, magnetite nanoparticles (MagNPs) consistently exhibit bactericidal effects across different types of bacteria. This study describes the synthesis, characterization, and antibacterial properties of magnetite MagNPs prepared by the coprecipitation method under continuous sonication. Scanning Electron Microscopy (SEM), X-ray Diffraction (XRD), and Dynamic Light Scattering (DLS) techniques revealed Fe3O4-NPs as spherical, uniform particles with an average size of approximately 16 nm. The antibacterial efficacy of MagNPs was investigated by combining them with methanolic extracts of three medicinal plants known for their antibacterial properties: Aloysia triphylla, Sarcopoterium spinosum, and Urtica pilulifera. The combined effect was assessed against both wild type and resistant strains of Staphylococcus aureus and Escherichia coli. The antibacterial synergistic effect of MagNPs and plant extracts was evaluated by the MIC test, which showed significant inhibitory properties against the growth of the four bacterial strains as compared to control samples of plant extracts alone. Furthermore, the synergistic effect of MagNPs combined with extracts from Rosmarinus officinalis, Anchusa azurea, Quercus infectoria, and Urtica pilulifera significantly prevented biofilm development in both sensitive and resistant strains of Staphylococcus aureus.
12 January 2002 in Journal of Macromolecular Science, Part A
A series of diaminecarbosilazane-containing polymers of the general formula [-SiPh2-NH-R-NH-]n, (R is 1,2-ethane, 1,3-propane, 1,4-butane, 1,6-hexamethylene and 1,4-phenylene) has been prepared by polycondensation of dichlorodiphenylsilane with the corresponding aliphatic and aromatic diamines in the presence of a weak base. These carbosilazane polymers were characterized by elemental analysis, thermogravimetric analysis (TGA), infrared (FT-IR), 1H NMR and electronic(UV-vis) spectroscopy. The average molecular weight and n value of these polymers were found to range from 6000 to 9500 and 20 to 37, respectively.
1 June 2003 in Journal of Inorganic and Organometallic Polymers and Materials
Intrinsically conducting polyaniline is grafted onto a preformed poly(styrene-co-maleanilic acid) copolymer backbone via chemical oxidative coupling of aniline in acidified chloroform/water emulsion. The structure and textural morphology of the grafted poly(S-co-MA-g-PANI) are examined by different spectroscopic, thermal, powder X-ray diffraction and scanning electron microscopic techniques. The d.c. electrical conductivity of the grafted emeraldine base of the obtained materials displays a d.c. conductivity of the order of 10−7 – 10−9 Scm−1, which is ∼2 orders of magnitude greater than that of the reported PANI-EB homopolymer. This enhancement in d.c. conductivity is explained in terms of microstructure-electronic conductivity relationship.
1 January 2008 in Journal of Solid State Chemistry