Neutron emission measurements, by means of ³He devices and neutron bubble detectors, were performed during three different kinds of compression tests on brittle rocks: (i) under displacement control, (ii) under cyclic loading and (iii) by ultrasonic vibration. The material used for the tests was Green Luserna Granite. Since the analyzed material contains iron, our conjecture is that piezonuclear fission reactions involving fission of iron into aluminum, or into magnesium and silicon, should have occurred during compression damage and failure. This hypothesis is confirmed by Energy Dispersive X-ray Spectroscopy (EDS) tests conducted on Luserna Granite specimens. It is also interesting to emphasize that the present natural abundances of aluminum (≈8%), and silicon (28%) and scarcity of iron (≈4%) in the continental Earth's crust should be possibly due to the piezonuclear fission reactions considered above.

Acoustic emissions (AE) due to microcracking in solid materials permit the monitoring of fracture processes and the study of failure dynamics. As an alternative method of integrity assessment, measurements of electrical resistance can be used as well. In the literature, however, many studies connect the notion of criticality with AE originating from the fracture, but not with the changes in the electrical properties of materials. In order to further investigate the possible critical behavior of fracture processes in rocks and cement-based materials, we apply natural time (NT) analysis to the time series of AE and resistance measurements, recorded during fracture experiments on cement mortar (CM) and Luserna stone (LS) specimens. The NT analysis indicates that criticality in terms of electrical resistance changes systematically precedes AE criticality for all investigated specimens. The observed greater unpredictability of the CM fracture behavior with respect to LS could be ascribed to the different degree of material homogeneity, since LS (heterogeneous material) expectedly offers more abundant and more easily identifiable fracture precursors than CM (homogenous material). Non-uniqueness of the critical point by varying the detection threshold of cracking events is apparently due to finite size effects which introduce deviations from the self-similarity.