This study sought to characterize aluminum nanocomposite wires that were fabricated through a cold-rolling process, having potential applications in TIG (tungsten inert gas) welding of aluminum. A206 (Al-4.5Cu-0.25Mg) master nanocomposites with 5 wt % γAl2O3 nanoparticles were first manufactured through a hybrid process combining semi-solid mixing and ultrasonic processing. A206/1 wt % γAl2O3 nanocomposites were fabricated by diluting the prepared master nanocomposites with a monolithic A206 alloy, which was then added to a pure aluminum melt. The fabricated Al–γAl2O3 nanocomposite billet was cold-rolled to produce an Al nanocomposite wire with a 1 mm diameter and a transverse area reduction of 96%. Containing different levels of nanocomposites, the fabricated samples were mechanically and electrically characterized. The results demonstrate a significantly higher strength of the aluminum wires with the nanocomposite addition. Further, the addition of alumina nanoparticles affected the wires’ electrical conductivity compared with that of pure aluminum and aluminum–copper alloys. The overall properties of the new material demonstrate that these wires could be an appealing alternative for fillers intended for aluminum welding.
11 April 2014 in Science and Engineering of Composite Materials
This study focuses on the fabrication of aluminum treated with nanocomposites made of aluminum and NbB 2 and ZrB 2 nanoparticles. These nanoparticles were obtained by fragmentation in a ball mill and then mechanically alloyed with pure aluminum powder to form Al/NbB 2 and Al/ZrB 2 nanocomposite pellets, which were then sintered at 260°C for half an hour to improve the metal/borides interface. The sintered nanocomposites were incorporated into molten pure aluminum to produce 1-mm-diameter wires after cold forming. The wire specimens were mechanically characterized and their electrical resistivity was measured. Our results demonstrated the feasibility of improving the mechanical properties of aluminum wires with the addition of nanocomposites without significantly affecting their electrical conductivity.
1 December 2015 in Journal of the Mechanical Behavior of Materials
This study hinges on the feasibility of strengthening Al and Al-Mg wires by adding Al nanocomposite pellets containing MgB 2 nanoparticles into the melt upon fabrication. These MgB 2 nanoparticles were obtained by fragmentation using a high-energy ball mill, and were, afterward, mechanically alloyed with pure aluminum. The resulting MgB 2 /Al nanocomposite pellets were sintered at 260°C to be subsequently added into molten aluminum and an Al-Mg alloy melt. Cold rolling intercalated with stepwise annealing allowed the fabrication of 1 mm diameter wires with a final area reduction of 96%. Mechanical and physical properties of the treated wire specimens were compared to those of similarly processed pure aluminum wire. The ultimate tensile strength of the treated wires increased approximately double fold with respect to untreated wires at the expense of some loss in electrical conductivity.
This research focuses on the fabrication of aluminum wires treated with MoB2 nanoparticles and their effect on selected mechanical and thermal properties of the wires. These nanoparticles were obtained by fragmentation in a high-energy ball mill and then mechanically alloyed with pure aluminum powder to form Al/MoB2 pellets. The pellets were added to molten pure aluminum (99.5%) at 760 °C. Afterwards, the treated melt was cast into cylindrical ingots, which were cold-formed to the desired final diameter with intermediate annealing. X-ray diffraction and optical microscopy allowed characterizing the structure and microstructure of the material. The wires underwent tensile and bending tests, as well as electrical measurements. Finally, this research demonstrated how the mechanical properties of aluminum wires can be enhanced with the addition of MoB2 nanoparticles with minimal effects on the material resistivity.
In Al-Mg alloys, the Portevin-Le Chatelier phenomenon, or dynamic strain aging, reveals itself as serrations upon plastic tensile deformation. This research evaluates this phenomenon when Al/NbB2 nanocomposite pellets are added to a magnesium-supersaturated Al matrix. A ball-milled 90 wt % Al and 10 wt % NbB2 nanocomposite helped inoculate an Al-Mg melt to incorporate the nanoparticles effectively. The melt was cast into rods that were cold-rolled into 1 mm diameter wires. Two sets were prepared: The first group was an as-cast set of samples, for comparison purposes, whereas the second was a solution-treated set. The solution treatment consisted of annealing followed by ice-water quenching. The results corroborating that the phenomenon was observable only in the specimens bearing the solution treatment, were used as the research baseline. Said treated alloy was compared to one containing the nanoparticles, which proved that the NbB2 particles caused a reduction of the serrated signal amplitude.
The Portevin-Le Chatelier (PLC) phenomenon or dynamic strain aging in Al–0.5 wt. % Mg alloys was investigated at different strain rates. This research also examined the effect of γAl2O3 nanoparticles on the PLC phenomenon. A nanocomposite made of A206/1.0 wt. % γAl2O3 was manufactured to this purpose and then, added to an Al–0.5 wt. % Mg melt to obtain ingots of Al–0.5 wt. % Mg–20 wt. % A206/1.0 wt. % γAl2O3 and Al–0.5 wt. % Mg–10 wt. % A206/1.0 wt. % γAl2O3 with 6 mm diameter. Cold deformation allowed manufacturing 1 mm diameter wires using the 6 mm diameter ingots. A 300 °C solution treatment, followed by rapid cooling in ice water permitted to retain Mg atoms in solid solution. The tensile tests performed on the wires revealed the PLC phenomenon upon the tensile stress vs. strain plastic zone. The phenomenon was quantified using MatLab™ and statistical analysis. The results demonstrated how the alumina nanoparticles can diminish the serration amplitude of the PLC phenomenon.