The use of warm-mix recycling technology can reduce the mixing temperature and the secondary aging of binders in reclaimed asphalt pavement (RAP), which is one of the effective ways to recycle high-content RAP. In this study, the penetration, softening point, ductility, and viscosity were used to characterize the conventional physical properties of aged asphalt after regenerating, while a dynamic shear rheometer (DSR), force ductility tester (FDT), and atomic force microscope (AFM) were used to evaluate the rheological performance and micro-morphology of aged asphalt incorporating a new bio-based warm-mix rejuvenator (BWR) and a commercial warm-mix rejuvenator (ZJ-WR). The regeneration mechanism of warm-mix rejuvenators on aged asphalt was analyzed by Fourier transform infrared spectroscopy (FTIR). The results show that the new bio-based warm-mix rejuvenator can restore the conventional physical properties, low-temperature performance, and micro-morphology of aged asphalt with an appropriate dosage, but it has a negative effect on high-temperature performance. In comparison with 2D area parameters, 3D roughness parameters were more accurate in evaluating the variation in micro-morphology of aged asphalt after regeneration. The FTIR analysis results indicate that both the new bio-based warm-mix rejuvenator and the commercial warm-mix rejuvenator regenerate aged asphalt by physical action, and A_S=O and A_C-H values are more reasonable than the A_C=O value for the restoration evaluation of aged asphalt. And the new bio-based warm-mix rejuvenator has a better regeneration effect on the performance and micro-morphology of aged asphalt than the commercial warm-mix rejuvenator.

To study the effect of aggregate type on the adhesion between asphalt and aggregate, limestone, basalt, diabase, and 70# asphalt with SBS asphalt were selected. The mineral phase composition of the aggregates was analyzed by X-ray diffraction. The surface energy theory was used to calculate the adhesion work and the work of flaking. The modified water boiling method combined with image processing technology was used to quantitatively characterize the flaking behavior of the asphalt. The results show that the aggregate type is closely related to the asphalt–aggregate adhesion. The mineral compositions of different types of aggregates vary significantly, with limestone, being a strongly alkaline aggregate predominantly comprising CaCO₃, exhibiting better adhesion with asphalt. The contact angle test and modified boiling method also yielded the same results, and the adhesion relationship with asphalt was limestone > basalt > diabase. Image processing technology effectively characterizes the spalling situation of asphalt and conducts quantitative analysis.

The blending degree between virgin asphalt and aged asphalt has a significant effect on road performance of reclaimed asphalt mixture. This study presented an innovative examination of blending behavior between virgin asphalt and aged asphalt incorporating a new bio-based warm-mix rejuvenator (BWR) by utilizing Atomic Force Microscopy (AFM). Through analyzing the variation of several micro-morphology parameters between virgin asphalt and aged asphalt (or recycled asphalt) after blending, an index of regenerative blending degree (RBD) was proposed to quantitatively evaluate their blending behavior, and the effect of various blending temperatures and durations on regenerative blending degree was investigated. The results show that the regenerative blending degree between virgin asphalt and aged asphalt was higher than that between virgin asphalt and recycled asphalt under the same blending condition. A clear linear correlation was observed between the regenerative blending degree calculated by 3D micro-morphology parameters and the dosage of bio-based warm-mix rejuvenator in recycled asphalt, with a correlation coefficient of 0.98. With the increase in blending duration, the regenerative blending degree between virgin asphalt and recycled asphalt increased first and then decreased, but continued to improve with the increase in blending temperature, which indicates that a higher blending temperature and prolonging the blending duration properly have a positive effect on the blending processing between virgin asphalt and recycled asphalt. Compared with the regenerative blending degree calculated by 2D micro-morphology parameters, the regenerative blending degree calculated by 3D micro-morphology parameters is more reasonable to quantify the blending behavior between virgin asphalt and recycled asphalt.