Xi Zou

Dr. Xi Zou


Research Focus & Metrics

Academic Career Length

3Years (2024-Present)

(Calculated once Scilit publication data is synced: current year − year of first publication + 1)

Representative Publications

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2 October 2024 in Materials
Verified
Journal Article
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MCManping Cheng
Manping Cheng
XZXi Zou
Xi Zou
TCTengfei Chang
Tengfei Chang
LLLehui Liu
Lehui Liu
In the process of directed energy deposition (DED), the grain structure of the deposited samples is determined by two aspects. The first is the initial solidification grain structure; the second is the effect of the upper thermal cycle on the solidified grain structure of the lower layer. Dynamic recrystallization and grain growth can be activated under suitable strain and the temperature resulting from thermal cycles. The evolution of grain size and the geometric dislocation density (GND) of austenitic stainless steel 316 L under different strains and temperatures caused by thermal cycles was investigated. It is found that dynamic recrystallization requires an appropriate level of accumulated strain, temperature, and initial grain size. Under <2% accumulated strain and 400–1200 °C conditions caused by 30 layers of thermal cycles, fully dynamic recrystallization occurs with coarse initial grains (CIG), leading to the complete coarsening of grains. However, relatively fine initial grains (FIG) under the same conditions only display partial dynamic recrystallization. The next 2–4% strain and 400–700 °C by 60 layers of thermal cycles make up the driving force of fully dynamic recrystallization, and the grains coarsen completely. Larger accumulated strain (4–6%) and lower temperature (400–600 °C) by 90 layers of thermal cycles and FIG provide more nucleation sites for dynamic recrystallization, which leads to little coarsening of grains even after fully dynamic recrystallization. Temperature, accumulated strain, and the amount of δ-ferrite promote the formation of sub-grains during dynamic recrystallization caused by thermal cycles, which leads to the increase in GND.

27 October 2024 in Materials
Verified
Journal Article
Open access
PDF file
ZYZhou Yan
Zhou Yan
JGJia Guo
Jia Guo
XZXi Zou
Xi Zou
SWSiyu Wang
Siyu Wang
Directed energy deposition with laser beam (DED-LB) components experience significant residual stress due to rapid heating and cooling cycles. Excessive residual tensile stress can lead to cracking in the deposited sample, resulting in service failure. This study utilized digital image correlation (DIC) and thermal imaging to observe the in situ temporal evolution of strain and temperature gradients across all layers of a deposited 316 L stainless steel thin wall during DED-LB. Both continuous-wave (CW) and pulsed-wave (PW) laser modes were employed. Additionally, the characteristics of thermal cracks and geometric dislocation density were examined. The results reveal that PW mode generates a lower temperature gradient, which in turn reduces thermal strain. In CW mode, the temperature–stress relationship curve of the additive manufacturing sample enters the “brittleness temperature zone”, leading to the formation of numerous hot cracks. In contrast, PW mode samples are almost free of cracks, as the metal avoids crack-sensitive regions during solidification, thereby minimizing hot crack formation. Overall, these factors collectively contribute to reduced residual stress and improved mechanical properties through the adjustment of pulsed-wave laser deposition.

20 December 2024 in Coatings
Verified
Journal Article
Open access
PDF file
MCManping Cheng
Manping Cheng
XZXi Zou
Xi Zou
TCTengfei Chang
Tengfei Chang
QCQi Cao
Qi Cao
HJHoulai Ju
Houlai Ju
ZWZhenxing Wu
Zhenxing Wu
Continuous-wave laser (CW) and pulsed-wave laser (PW) are the two laser modes in direct energy deposition (DED). This paper mainly reports on a study into the effects of the two laser modes on residual stresses with a given energy input. The contour method (CM) with non-uniform spatial distribution of inspection points was used to capture residual stress distributions in DED of Fe3000 on a substrate made of 316L stainless steel. Residual stresses in the transition zone between the deposit and the substrate were carefully examined to gain an understanding of cracks frequently observed at the connection between the substrate and the deposit. Furthermore, X-ray diffraction, along with successive material removal, was used to reveal residual stresses at various depths in the substrate. The results showed that significant tensile longitudinal stresses developed at the substrate–deposit junction for both CW and PW laser modes. It increased sharply (about 64%) with the increase in energy input for CW mode, while it showed the opposite trend for PW mode; the longitudinal residual stress decreased 13.2% with the increase in energy input. PW, however, introduced lower residual stress than that of CW under the condition of high-energy input; the maximum longitudinal residual stress decreased by about 10.4% compared to CW mode. This was due to stress relaxation at high-energy inputs in PW mode. In addition, residual stresses were found to be higher than the initial yield stress, and yielding occurred in the deposited part. The results determined by the CM and X-ray diffraction depth profiling were found to be consistent.

12 February 2025 in Coatings
Verified
Journal Article
Open access
PDF file
MCManping Cheng
Manping Cheng
XZXi Zou
Xi Zou
MGMuhong Gong
Muhong Gong
TCTengfei Chang
Tengfei Chang
QCQi Cao
Qi Cao
HJHoulai Ju
Houlai Ju
In this paper, 316 L stainless steel deposited samples were fabricated by direct layer deposition (DED) using both continuous-wave (CW) and pulsed-wave (PW) laser modes. Effects of laser modes on residual stress of deposited samples were investigated. On this basis, a mathematical model of thermal stress evolution during DED was established for the first time based on the energy equation. The variation law of thermal stress on the top of the substrate under multi-material and multi-process conditions was qualitatively predicted and the corresponding residual stress reduction mechanism has been studied using this model. Meanwhile, in situ thermal strain evolution is used to prove the correctness of the mathematical model. This model lays the foundation for predicting the thermal stress evolution and the magnitude of the residual stress of deposited samples under multi-material and process conditions during DED.

3 July 2025 in Coatings
Verified
Journal Article
Open access
PDF file
MCManping Cheng
Manping Cheng
XZXi Zou
Xi Zou
YZYuan Zhu
Yuan Zhu
TCTengfei Chang
Tengfei Chang
QCQi Cao
Qi Cao
LQLijun Qiang
Lijun Qiang
In the Direct Energy Deposition (DED) process, the deposited material experiences intricate thermo-mechanical processes. Subsequent thermal cycling can trigger Dynamic Recrystallization (DRX) under suitable conditions, with specific strain and temperature parameters facilitating grain refinement and homogenization. While prior research has examined the impact of thermal cycling in continuous wave (CW) lasers on DRX in 316 L stainless steel deposits, this study delves into the effects of pulsed wave (PW) laser thermal cycling on DRX. Here, the thermo-mechanical response to PW cyclic thermal loading is empirically assessed, and the evolution of microstructure, grain morphology, geometric dislocation density (GND), and misorientation map during PW DED of 316 L stainless steel is scrutinized. Findings reveal that DRX is activated between the 8th and 44th thermal cycles, with temperatures fluctuating in the range of 680 K–750 K–640 K and grains evolving within a 5.6%–6.2%–5.2% strain range. After 90 thermal cycles, the grain microstructure undergoes significant alteration. Throughout the thermal cycling, dynamic recovery (DRV) occurs, marked by sub-grain formation and low-angle grain boundaries (LAGBs). Continuous dynamic recrystallization (CDRX) accompanies discontinuous dynamic recrystallization (DDRX), with LAGBs progressively converting into high-angle grain boundaries (HAGBs). Elevated temperatures and accumulated strain drive dislocation movement and entanglement, augmenting GND. The study also probes the influence of frequency and duty cycle on grain microstructure, finding that low pulse frequency spurs CDRX, high pulse frequency favors DRV, and the duty cycle has minimal impact on grain microstructure under PW cyclic thermal load.