A thorough investigation of the viability of rice starch conjugation with three different phenolic compounds—gallic acid, sinapic acid, and crude Mon-pu (Glochidion wallichianum Muell Arg) (MP) extract—was conducted using a variety of developed methods which modified the techno-functionality and digestibility of the end product. With and without the aid of ultrasonication (US), phenolic compounds were complexed with hydrothermally pre-gelatinized rice starch prepared using distilled water or plasma-activated water (PAW). The in vitro digestibility, structural features, rheological and thermal properties, and in vitro antioxidant activity of starch–phenolic complexes were evaluated. The US-assisted starch–MP complex in water had the highest complexing index (CI) value (77.11%) and resistant starch (RS) content (88.35%), resulting in a more compact and stable ordered structure. In all complexes, XRD revealed a new minor crystalline region of V-type, which was stabilized by hydrogen bonding as defined by FTIR and H1-NMR. Polyphenols caused a looser gel structure of starch, as imaged by a scanning electron microscope (SEM). Starch–phenolic complexes outperformed other complexes in terms of in vitro antioxidant activity. Gallic acid addition to starch molecules boosted DPPH scavenging activity, notably when synthesized in PAW regardless of US assistance, although having lower CI and RS values than the MP complex. Therefore, this research lays the groundwork for the efficient production of functional food ingredients based on rice starch and polyphenols.
The potential of microwave drying in the production of rehydrated foods is demonstrated with stink beans (Parkia speciosa), smelly legumes of Africa and Asia. Compared to stink beans dehydrated by convective drying and freeze drying, the microwave products exhibit higher moisture contents, but the distribution of microscopic pores leads to good rehydration characteristics. Dehydration by microwave drying is also achieved within a much shorter period than that commonly used in freeze drying. The dehydration time can be further reduced to 6 h comparable to convective drying, and the moisture content is dropped to 11% by decreasing the pressure during microwave drying. However, the rehydration time remains around 65 min for products from both ambient and low-pressure (400 Pa) microwave drying. In rehydration, the period is successfully reduced to 30 min by increasing the water temperature to 70 °C. The results indicate that microwave drying does not affect the value of crude protein and rehydrated products are comparable to fresh stink beans. From these findings, the microwave drying technique is an applicable technology for both manufacturers and consumers, with acceptable drying time and rehydration characteristics.
10 May 2024 in Plasma Chemistry and Plasma Processing