The microencapsulation of tea and herbal extracts is gaining considerable attention in the food industry, particularly in the production of instant powders. This review examines the application of spray-drying and freeze-drying technologies for the encapsulation of bioactive compounds, focusing on the role of wall materials. Over the past two decades, carbohydrate-based (e.g., maltodextrin), gum-based (e.g., gum Arabic), and protein-based (e.g., whey protein isolate) materials have been widely used due to their impact on sensory properties, stability, protection of bioactive compounds, and other critical attributes of encapsulated products. Despite their widespread use, these materials have distinct advantages and limitations, such as cost, availability, and compatibility with different extracts. This review provides a comprehensive analysis of their physical and chemical properties, examines alternative and emerging wall materials (e.g., beta-cyclodextrin, sodium alginate, and inulin), and highlights the potential of combining different materials to optimise encapsulation outcomes. It also identifies current research gaps and future directions to improve the efficacy and quality of encapsulated tea and herbal powders.

Microencapsulation of extra virgin olive oil has been taken into consideration. Initially, emulsions were prepared using extra virgin olive oil and aqueous solutions of different proportions of maltodextrin (MD) having dextrose equivalent (DE) 19 and whey protein isolates (WPI), such as 100% MD, 100% WPI, 25% MD + 75% WPI, 50% MD + 50% WPI and 75% MD + 25% WPI. Subsequently, emulsions were used for dehydration by either spray-drying (SD) or freeze-drying (FD) to produce olive oil microcapsules. Emulsion stability, viscosity and droplet size influenced the characteristics of the microcapsules. The highest encapsulation efficiency was achieved using 50% MD + 50% WPI in the emulsions with subsequent SD. The moisture content of the microcapsules increased with increasing proportions of MD. The size of the microcapsules increased with increasing proportions of WPI. The bulk density and tapped density were reduced with higher proportions of MD in the microcapsules. Furthermore, microcapsules with a higher proportion of MD exhibited poor flowability and high cohesiveness. Microcapsules from the higher proportion MD emulsions, followed by SD were spherical with a smooth surface; however, microcapsules with dent structures were produced from 100% WPI in the emulsions with subsequent SD. Microcapsules, produced from emulsions with a higher proportion of WPI, followed by FD were flat flakes and had irregular surfaces.

This study investigates the drying behavior of three polyamide-based 3D printing filaments (PA6-GF, PA6-CF, and PPA-CF) under varying temperature conditions. A comparative approach was applied using both segment-based and spool-based drying experiments. Moisture loss was recorded at 70 °C, 95 °C, and 120 °C, and the drying kinetics were modeled using a four-parameter logistic (4PL) function. Results revealed temperature-dependent differences in the drying rates and equilibrium moisture levels, with PPA-CF exhibiting the highest thermal resistance. The segment-based measurements enabled a precise kinetic evaluation, while the spool-based tests provided insights into real-world drying performance using hobbyist equipment. This study highlights that, while all three filaments benefit from pre-drying, optimal conditions vary significantly depending on the polymer matrix and reinforcement. The proposed 4PL-based modeling approach proved effective for characterizing the moisture removal process and can support improved drying protocols prior to fused filament fabrication. These findings contribute to a better understanding and optimization of filament conditioning practices in additive manufacturing.