Dual-scale (nano and micron) particle-reinforced TiB2/6061Al matrix composites with different contents of TiB2 were prepared using powder metallurgy, and then analyzed via microstructure observation and tests of microhardness, tensile properties, and friction and wear properties. The 6061Al powders’ particles changed from spherical to flaky after two rounds of high-energy ball milling, and the TiB2 enhancer was embedded in or wrapped by the matrix particles after high-energy ball milling. Metallurgical bonding between TiB2 particles and the matrix was achieved, and Al3Ti was synthesized in situ during sintering. The hot-pressing process eliminated the internal defects of the composites, and the TiB2 particles were diffusely distributed in the matrix. The best comprehensive mechanical properties (hardness and tensile strength) were achieved when the mass fraction of TiB2 was 5% (1% micron + 4% nano); the hardness and tensile strength of the composites reached 131 HV and 221 MPa—79.5% and 93.9% higher than those of the pure matrix, respectively. The composites’ average coefficient of friction and volumetric wear rate were reduced. Composites with a TiB2 mass fraction of 7% (3% micron + 4% nano) had the highest average coefficients of friction and the lowest volumetric wear rate of 0.402 and 0.216 mm3∙N−1∙m−1, respectively. It was observed that adhesion influences the friction mechanism, which transitions from adhesive wear with slight oxidative wear to abrasive wear.
1 November 2023 in Materials Science and Technology
Friction stir lap welding experiments between 6061 aluminum alloy and DP590 dual-phase steel plates were carried out. The effects of welding parameters and the addition of Cu foil interlayers with 0–0.3 mm thickness on the microstructures and mechanical properties of the lap joints were investigated. The shear strength of the joint reached the maximum value of 5337 N and showed a mixed ductile-brittle fracture mode when the welding speed, the rotating speed, and the thickness of the Cu foil intermediate layer were set to 80 mm/min, 900 rpm, and 0.1 mm, respectively. The plastic Al2Cu and AlCu intermetallic compounds formed through Al and Cu reaction at the aluminium alloy/steel interface play a beneficial role in the Cu-added joint strength.
Curvature effects are typically present in the process of additive manufacturing (AM), particularly for wire arc additive manufacturing. In this paper, stainless-steel wire was adopted to deposit thin-walled samples with different curvatures. Optical microscopy, SEM, EDS and micro-hardness was used to analyse the microstructure, composition and properties of the samples. The result shows that the bottom region of the thin-walled sample had a mainly planar and cellular crystal microstructure. For the middle region, the microstructure revealed mainly dendrites, and the top layer has equiaxed dendrite morphology. The microhardness value of the bottom was greater than that of the middle, and the microhardness value of the middle was greater than that of the top. Moreover, the grain size of the inner part (direct to curvature radius) was larger than that of the outer part, and the micro-hardness value exhibited an increasing tendency from the inner to the outer side. With enlarging curvature, the degree of grain size differences and micro-hardness variants decreased. Finally, an investigation with a low carbon steel wire showed that it had a similar curvature effect for its AM specimen.
In this study, FSW experiments were conducted on a 4 mm-thick A380 aluminium alloy plate and 6061 aluminium alloy using four different needle lengths (2.5 mm, 2.8 mm, 3.0 mm, and 3.5 mm) of H13 steel. The experiments were conducted at the same welding parameters (1000 rpm and 120 mm/min) to explore the effects of different stirring needle lengths on the microstructures and properties of the FSW joints. The experimental results show that FSW joints with varying lengths of needles have a significant effect on the microstructures and properties of welded joints, and the tensile strength increases and then decreases with increases in the needle length. A 2.8 mm needle length can achieve the maximum tensile strength of 203 MPa, about 85.3% of the base material. Too long or too short a needle leads to a decrease in joint performance. Furthermore, different needle lengths have a significant influence on the flowability of the weld core zone, and a suitable needle length will lead to better flowability in the weld core zone. With increases in the needle length, the heat production also increases, and the area of the RS-HAZ will increase with the heat production. When the joints achieve appropriate heat production, the weld core zone will experience grain refinement. At the same time, the grain will grow in the RS-HAZ; the hardness cloud diagram shows that, in the RS-HAZ, the material properties are weaker, and the tensile specimens are mainly fractured in the RS-HAZ. Finally, the tensile specimens exhibit mixed fracture.
Al2O3-TiC/6061Al composites were fabricated via in situ powder metallurgy using 6061 Al, TiO2, and graphite powders as starting materials. The effects of sintering temperature and ceramic particle content on the microstructure and mechanical properties of the composites were investigated. The wear performance of composites sintered at 1200 °C with varying ceramic particle content was also examined. The results indicate that the microstructure of the composite varied with the sintering temperature. At 1000 °C and 1100 °C, the microstructure primarily consisted of Al3Ti, Al2O3, and TiC phases. At 1200 °C and 1250 °C, the microstructure was predominantly composed of Al2O3 and TiC phases. The 6061 Al-12% (TiO2 + C) composite sintered at 1200 °C exhibited a tensile strength of 246 MPa, an elongation of 12.7%, and a microhardness of 104.2 HV0.1. Regarding wear performance, the wear behavior of the composites under different loads at 1200 °C was studied. Under a 30 N load, the 6061 Al-12% (TiO2 + C) composite demonstrated the lowest friction coefficient and wear rate, measured at 0.253 and 0.396 mm3·N−1·m−1, respectively. Analysis of the worn surface morphology under a 30 N load indicates that the dominant wear mechanism for the 6061 aluminum alloy is delamination wear, whereas for the 6061 Al-12% (TiO2 + C) composite, it is primarily abrasive wear.
15 September 2025 in Journal of Materials Engineering and Performance