This study aimed to produce activated carbon from desilicated rice husks using various carbonization and activation methods, including a tube furnace, muffle furnace, and artisanal pyrolysis. The resulting activated carbons were characterized for their adsorptive capacity through the determination of iodine number and methylene blue adsorption; these are key indicators of specific surface area and adsorbent quality. Advanced characterization techniques were employed, such as scanning electron microscopy (SEM), which revealed a highly porous and irregular surface structure, and energy dispersive X-ray spectroscopy (EDS), confirming the effective removal of impurities and optimization of the elemental composition. Atomic force microscopy (AFM) demonstrated favorable surface roughness for adsorption processes. Among the samples, CaDH162-CADH53 exhibited the highest performance, with an iodine number of 1094.8 mg/g and a yield of 93.5%, signifying a high adsorption capacity. The activation treatments with phosphoric acid and calcium carbonate significantly improved the porous structure, further enhancing the material’s adsorptive properties. In conclusion, the activated carbons produced in this study demonstrated optimal physicochemical properties for water purification and contaminant treatment applications. These findings highlight the potential of using agricultural waste, such as rice husk, as a sustainable and scalable alternative for industrial-scale activated carbon production.

This study focused on the comprehensive characterization of the adsorbent obtained from rice husk, which was selected for its high adsorption capacity in iodine solution (IS) and methylene blue solution (MBS). This was achieved with adsorbents prepared by a combined treatment involving calcium carbonate prior to carbonization and activation with phosphoric acid. Characterization was performed using advanced techniques, such as scanning electron microscopy (SEM), atomic force microscopy (AFM), laser light diffraction and energy-dispersive X-ray spectroscopy (EDS), which allowed for the evaluation of the adsorbent’s microstructure and composition. The results revealed a complex structure of the adsorbents with interconnected pores, which facilitates efficient adsorption in IS and MBS and the standard indicators to evaluate adsorption capacity. The novelty of this study lies in the application of advanced characterization techniques to optimize the adsorbent properties and understand how preparation conditions affect the adsorbent’s microstructure. The characterized adsorbent materials in this study presented great potential for applications in water treatment and industrial processes, offering an economical and environmentally sustainable solution. Promoting the use of rice husks in the production of adsorbents contributes to the circular economy, reducing production costs and environmental pollution. The results suggested that these materials are effective in the removal of pollutants, which make them relevant for practical applications in water and soil bioremediation.