To achieve enhanced surface characteristics in wire electrical discharge machining (WEDM), the present work reports the use of an artificial neural network (ANN) combined with a genetic algorithm (GA) for the correlation and optimization of WEDM process parameters. The parameters considered are the discharge current, voltage, pulse-on time, and pulse-off time, while the response is fractal dimension. The usefulness of fractal dimension to characterize a machined surface lies in the fact that it is independent of the resolution of the instrument or length scales. Experiments were carried out based on a rotatable central composite design. A feed-forward ANN architecture trained using the Levenberg-Marquardt (L-M) back-propagation algorithm has been used to model the complex relationship between WEDM process parameters and fractal dimension. After several trials, 4-3-3-1 neural network architecture has been found to predict the fractal dimension with reasonable accuracy, having an overall R-value of 0.97. Furthermore, the genetic algorithm (GA) has been used to predict the optimal combination of machining parameters to achieve a higher fractal dimension. The predicted optimal condition is seen to be in close agreement with experimental results. Scanning electron micrography of the machined surface reveals that the combined ANN-GA method can significantly improve the surface texture produced from WEDM by reducing the formation of re-solidified globules.

Ni–B alloys deposited by the electroless method are considered to be hard variants of the electroless nickel family. Inclusion of Mo or W to form ternary alloys improves the thermal stability of electroless nickel coatings. Therefore, in the present work, Ni–B, Ni–B–Mo, and Ni–B–W coatings are deposited; and their tribological behavior at room and high temperatures are investigated. Electroless Ni–B, Ni–B–Mo, and Ni–B–W coatings are deposited on AISI 1040 steel substrates. The coatings are heat treated to improve their mechanical properties and crystallinity. Tribological behavior of the coatings is determined on a pin-on-disc type tribological test setup using various applied normal loads (10–50 N) and sliding speeds (0.25–0.42 m/s) to measure wear and coefficient of friction at different operating temperatures (25 °C–500 °C). Ni–B–W coatings are observed to have higher wear resistance than Ni–B or Ni–B–Mo coatings throughout the temperature range considered. Although for coefficient of friction, no such trend is observed. The worn surface of the coatings at 500 °C is characterized by lubricious oxide glazes, which lead to enhanced tribological behavior compared with that at 100 °C. A study of the coating characteristics such as composition, phase transformations, surface morphology, and microhardness is also carried out prior to tribological tests.

The present work investigates the tribological behavior of electroless Ni-B coating in its as-plated condition at elevated operating temperatures. Ni-B coating is deposited using an electroless method on AISI 1040 steel specimens. Coating characterization is done using scanning electron microscopy, energy-dispersive X-ray analysis, and X-ray diffraction techniques. Vicker's microhardness and surface roughness are measured. Friction and wear tests are carried out on a pin-on-disc tribological test setup at room and elevated temperatures of 100, 300, and 500°C. The tribological behavior deteriorates at 100°C compared to room temperature. Electroless Ni-B coating shows excellent wear resistance at 300°C, which again degrades at 500°C due to severe oxidation and softening of the deposits. The worn surface of the coatings is analyzed using optical microscopy and scanning electron microscopy. Within the temperature range considered, the wear mechanism changes from adhesion to a combination of adhesion and abrasion as the temperature rises from ambient condition to 100°C, following which the wear mechanism is predominantly abrasive. The formation of a tribochemical oxide film also affects the tribological behavior of the coatings at high temperature.

Pitting corrosion and susceptibility to chloride attacks are the shortfalls of reinforcement steel used in concrete structures. The present work proposes the deposition of electroless nickel coatings to provide barrier protection due to their proven corrosion resistance. The effect of deposition of Ni–P, Ni–P–W and Ni–P–Cu coatings on the corrosion behavior of Fe—600 grade rebars in 3.5% NaCl has been investigated with the aid of potentiodynamic polarization and electrochemical impedance spectroscopy. The corrosion potential of bare rebar was observed to be −653 mV while that of electroless Ni–P, Ni–P–W and Ni–P–Cu coatings was −436, −391 and −356 mV respectively. The corrosion current density of the rebars also decreased significantly by the application of electroless nickel coatings. Nyquist plots also revealed a bigger semicircular loop for the coated rebars. The chloride attack was severe on the bare uncoated rebar and scanning electron micrograph revealed severe cracking. On the other hand, the vulnerability of the electroless coated rebars to pitting corrosion decreased greatly.