This study investigates the impact of hard coatings on the fatigue properties of pure titanium. A specialized fatigue test which ensured machine equivalence was conducted to compare the fatigue behavior of coated and uncoated metals. The findings reveal that the application of coatings adversely affects the fatigue properties of pure titanium due to stress concentration from the coating, which accelerates fatigue crack propagation within the substrate material. Notably, zigzag fatigue cracks at the interface between the coating and substrate and multiple micro-cracks initiated within the coating are found.
31 July 2017 in Metallurgical and Materials Transactions A
The effect of aging time on the crushing performance of Al-0.5Mg-0.4Si alloy used for safety components of automobile was investigated by tensile test and crush test. Moreover, the microstructure of the alloy was investigated by transmission electron microscopy (TEM). The results show that the localized deformation ductility index, ΔAabs, which is defined as the difference between total elongation and uniform elongation, of Al-0.5Mg-0.4Si alloy is 6.5%, 7.0% and 8.5%, respectively, after being aged at 210 °C for 1, 3 and 6 h, and this tendency is the same as that of the crushing performance. The spacing of grain boundary precipitates (GBPs) from TEM results are found to be 94.9, 193.6 and 408.2 nm after being aged at 210 °C for 1, 3 and 6 h, respectively, and this tendency is same to that of ΔAabs. A mechanism about the relation between the spacing of GBPs and the ductility index ΔAabs has been proposed based on localized deformation around GBPs. With the increase of GBPs spacing, the ΔAabs increases, and the crushing performance is improved.
This paper investigates the effect of retrogression time on the fatigue crack growth of a modified AA7475 aluminum alloy. Tests including tensile strength, fracture toughness, and fatigue limits were performed to understand the changes in properties with different retrogression procedures at 180 °C. The microstructure was characterized using scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The findings indicated that as the retrogression time increased, the yield strength decreased from 508 MPa to 461 MPa, whereas the fracture toughness increased from 48 MPa√m to 63.5 MPa√m. The highest fracture toughness of 63.5 MPa√m was seen after 5 h of retrogression. The measured diameter of η’ precipitates increased from 6.13 nm at the retrogression 1 h condition to 6.50 nm at the retrogression 5 h condition. Prolonged retrogression also increased the chance of crack initiation, with slower crack growth rate in the long transverse direction compared to the longitudinal direction. An empirical relationship was established between fracture toughness and the volume fraction of age-hardening precipitates, with increasing number density of precipitates seen with increasing retrogression time.
The hot-deformation behavior of three medium-strength Al-Zn-Mg alloys with different Zn/Mg ratios was studied using isothermal-deformation compression tests; the true strain and true stress were recorded for constructing series-processing maps. A few constitutive equations describe the relationship between flow stress and hot-working parameters. The microstructures were characterized using an electron backscatter diffraction (EBSD) detector and transmission electron microscope (TEM). The results show that the optimized deformation parameters for ternary alloy AA7003 are within a temperature range of 653 K to 813 K and with strain rates lower than 0.3 S−1. The microstructures show that materials with a lower Zn/Mg ratio of 6.3 could lead to a problematic hot-deformation capability. Alloys with a higher Zn/Mg ratio of 10.8 exhibited better workability than lower Zn/Mg ratios. The Al3Zr dispersoids are effective in inhibiting the recrystallization for alloy AA7003, and the Zn/Mg ratios could potentially affect the drag force of the dispersoids.