Conductive particles are one of the most important defects which can greatly degrade the performance of gas-insulated metal-enclosed switchgear (GIS). Many efforts have been made to clarify the influence on the withstand voltage, understand the flashover mechanism, and build a comprehensive model to describe the particle-initiated flashover. In this study, a partial discharge (PD) signal detected through a photomultiplier (PMT) and recorded by a high-speed data acquisition (DAQ) system was used to analyze the discharge development of a conductive particle-contaminated GIS insulator under constant high AC voltage. An additional PMT was used as a reference to eliminate the dark count of the PMT and the data collection method of a DAQ system was optimized to capture the pulse waveform of each PD to obtain detailed physical information. Spectra of the PD pulse amplitude over pulse width, PD counts within various amplitude ranges over time and phase resolved partial discharge (PRPD) patterns of the PDs in different stages are obtained through the captured PD waveforms. Characteristics of the PDs from the application of the high AC voltage up to the flashover of the insulator were then analyzed, and it was found that the features of the PDs in the near-flashover stage were significantly different to the previous stages.
The high density and controllability of radio frequency (RF)-biased inductively coupled plasma offer significant potential for diamond-like carbon (DLC) deposition on alumina. However, the effects of power and atmospheric parameters on DLC deposition have been understudied due to multiple constraints, such as discharge conditions and carbon source requirements. In this study, considering the dual requirements of ion flux and ion kinetic energy for deposition, an RF-biased inductively coupled plasma-enhanced DLC deposition method was proposed. A total of 273 deposition experiments designed by response surface methodology were performed over wide parameter ranges to explore the influence of atmospheric parameters, such as gas pressure and Ar/H2 auxiliary gas fractions, on feasible power. The results showed that there was a power threshold for DLC deposition on alumina, which increased with gas pressure and slightly decreased with auxiliary gas addition. The effect of auxiliary gas on DLC deposition exhibited duality due to changes in the dominance of ion etching and methane dissociation. The feasible power region for DLC deposition in multicomponent atmosphere was jointly constrained by the power threshold and etching action. This research contributed to the DLC modification of alumina substrate in batches.
13 March 2023 in Journal of Physics D: Applied Physics
Diamond-like carbon (DLC)-modified alumina microparticles are expected to be an ideal filler that can greatly improve the thermal conductivity of epoxy-alumina composites with a high fill factor, while the composites can still maintain high dielectric properties. Plasma-enhanced chemical vapor deposition (PECVD) has been mostly used to prepare DLC film on bulk material, and the ion energy in the plasma shows a crucial influence on the properties of the DLC. However, the properties of the DLC on solid microparticles prepared through the PECVD method as well as the effect of the ion energy are still unclear. In this paper, DLC on alumina microparticles has been prepared through a highly efficient method of repeated pulsed hollow cathode discharge in methane gas, and the characteristics of the DLC on the alumina particles have been studied and analyzed. The morphology and bond composition of DLC on particles have been studied through electron microscopy, Raman spectrometer and x-ray photoelectron spectroscopy. The ion energy distribution in the discharge plasma was diagnosed and used to analyze its effect on the hybrid bond content of the DLC through correlation analysis. The correlation of the ion energies and the hybrid bond content of the DLC shows that hydrocarbon ions in the discharge plasma with an energy of 100–200 eV present the most benefit to the formation of the sp3 hybrid bond content of DLC film on alumina microparticles. In addition, hydrogen ions with an energy of 700–1000 eV are also beneficial to improve the sp3 hybrid bond content of the DLC film.
The ability to manipulate ion energy is crucial for the practical implementation of pulsed hollow cathode discharge in plasma deposition. This paper presents a method for generating plasma through double pulse voltage superposition, which excites the hollow cathode discharge. By superimposing a high-amplitude pulse with a narrow width and a low-amplitude pulse with an extended width, gas ionization and ion acceleration can be stimulated respectively. With this approach, relative independent control over ion flux density and ion energy becomes possible. Increasing the amplitude of the narrow pulse enhances the ion flux density, while increasing the amplitude of the long pulse boosts average ion energy.
1 September 2024 in Review of Scientific Instruments
Depositing diamond-like carbon (DLC) film is considered to be more promising for surface modification of microparticles. The development of reliable and precise measurement techniques for DLC coatings on microparticles is crucial for advancing research in this field. This paper introduces a methodological approach for quantifying the thickness of the film on microparticles. The thickness of the film is obtained by establishing the quantitative relationship between the energy lost when electrons pass through the film and the thickness of the film. The proposed method allows for the estimation of film thickness by assessing solely the elemental abundance on the particle surfaces.