Synthetic polygranular graphites have a wide range of current and potential applications. Indeed, some are being considered as candidate moderator materials for the next generation of nuclear power plants, which are designed to operate at temperatures as high as 1000 °C. Detailed experimental work has been performed to investigate the electrical resistivity and mechanical behaviour of a synthetic graphite over a range of temperatures. An electrothermomechanical testing rig has been employed to conduct tensile tests to evaluate elastic modulus and fracture strength over the temperature range from room temperature to 700 °C for a near-isotropic synthetic polygranular graphite. A series of mm length scale ‘dogbone’ geometry specimens, containing varying levels of porosity between 8% and 18%, were used for testing. Acquired data revealed an average of 30% gain in material stiffness, occurring at temperatures above 400 °C. Tensile strength decreased linearly with increasing porosity at higher temperatures (700 °C). The accumulated percentage reduction of resistivity during the transition from room temperature to 700 °C reduced linearly with increasing amounts of porosity. The resistivity and mechanical property measurements are discussed, with particular attention given to the porosity of the synthetic graphite.

Background: The potential effect of image noise artefacts on Digital Volume Correlation (DVC) analysis has not been thoroughly studied and, more particularly quantified, even though DVC is an emerging technique widely used in life and material science over the last decade. Objective: This paper presents the results of a sensitivity study to shed light on the effect of various noise artefacts on the full-field kinematic fields generated by DVC, both in zero and rigid body motion. Methods: Various noise artefacts were studied, including the Gaussian, Salt & Pepper, Speckle noise and embedded Ring Artefacts. A noise-free synthetic microstructure was generated using Discrete Element Modelling (DEM), representing an idealistic case, and acting as the reference dataset for the DVC analysis. Noise artefacts of various intensities (including selected extreme cases) were added to the reference image datasets using MATLAB (R2022) to form the outline of the parametric study. DVC analyses were subsequently conducted employing AVIZO (Thermo Fisher). A subset-based local approach was adopted. A three-dimensional version of the Structural Similarity Index Measure (SSIM) was used to define the similarity between the compared image datasets on each occasion. Sub-pixel rigid body motion was applied on the DEM-generated microstructure and subsequently “poisoned” with noise artefacts to evaluate mean bias and random error of the DVC analysis. Results: When the local approach is implemented, the sensitivity study on zero motion data revealed the insignificant effect of the Gaussian, Salt & Pepper, and Speckle noise on the DVC-computed kinematic field. Therefore, the presence of such noise artefacts can be neglected when DVC is executed. On the contrary, Ring Artefacts can pose a considerable challenge and therefore, DVC results need to be evaluated cautiously. A linear relationship between SSIM and the correlation index is observed for the same noise artefacts. Gaussian noise has a pronounced effect on the mean bias error for sub-pixel rigid body motion. Conclusions: Generating synthetic image datasets using DEM enabled the investigation of a variety of noise artefacts that potentially affect a DVC analysis. Given that, any microstructure – resembling the material studied – can be simulated and used for a DVC sensitivity analysis, supporting the user in appropriately evaluating the computed kinematic field. Even though the study is conducted for a two-phase material, the method elaborated in this paper also applies to heterogeneous multi-phase materials also. The conclusions drawn are valid within the environment of the AVIZO DVC extension module. Alternative DVC algorithms, utilising different approaches for the cross-correlation and the sub-pixel interpolation methods, need to be investigated.