In this work, well-designed zinc oxide-reduced graphene oxide (ZnO-rGO) nanorods (NRs) were synthesized by a hydrothermal method using electrospun ZnO-rGO seed layers. The ZnO-rGO seed layers were fabricated on fluorine-doped tin oxide (FTO) glass substrates through calcined of electrospun nanofibers at 400 °C in the air for 1 h. The nanofibers were prepared by electrospinning different spinning voltages and a spinning solution containing zinc acetate, polyvinyl pyrrolidone, and 0.2 wt% rGO. From a detailed characterization using various analytical techniques, for instance, X-ray diffraction (XRD), field emission scanning electron microscopy (SEM), Raman spectroscopy, photoluminescence (PL), and X-ray photoelectron spectroscopy (XPS), the dependence of the structure, morphology, and optical properties of the ZnO-rGO NRs was demonstrated. The photocatalytic activities of ZnO-rGO nanorods were evaluated through the degradation of dye methyl orange (MO). The results show that the change of spinning voltages and the coupling of rGO with ZnO improved photodecomposition efficiency as compared to pure ZnO. The highest photocatalytic efficiency was obtained for the ZnO-rGO NRs prepared with a spinning voltage of 40 kV.

Polyvinyl alcohol (PVA) nanofibers reinforced with multi-walled carbon nanotubes (MWCNTs) were fabricated by electrospinning. MWCNTs were introduced into the PVA matrix through the application of an electric field. The morphology of the composite MWCNTs/PVA fibers was characterized by scanning electron microscopy. Results show that the nanofibers had a diameter between 48 and 103 nm and contained a variable amount of MWCNTs. The electrical properties of MWCNTs/PVA nanofibers were investigated by fabricating impedance-type sensors. The impedance and electrical conductivity of the samples were evaluated in the range 46% and 89% relative humidity

In the present work, a TiO₂/zeolite photocatalyst was synthesized by dispersing TiO₂ nanoparticles obtained through the sol-gel method onto the surface of natural zeolite derived from ignimbrite residue. The zeolite was obtained from an ignimbrite rubble treatment collected from a quarry in Arequipa City, Peru. The research focused on the effect of zeolite on the TiO₂ nanoparticles. The synthesized photocatalysts were characterized using various techniques, including field-emission scanning electron microscopy (FE-SEM), energy-dispersive X-ray (EDS), X-ray diffraction (XRD), diffuse reflectance spectroscopy (DRS), and Brunauer–Emmett–Teller surface area analysis (BET). The results revealed that the TiO₂/zeolite samples displayed high crystallinity, with TiO₂ being present in three phases and zeolite being present in the analcime phase. Furthermore, these samples exhibited a band gap of 3.14 eV and a high surface area compared to that of bare TiO₂. Finally, the photocatalytic activity of the TiO₂/zeolite composite obtained was evaluated toward the decomposition of 10 ppm and 20 ppm of methyl orange (MO) dye. The TiO₂/zeolite samples demonstrated improved photocatalytic activity compared to that of pristine TiO₂ under the same experimental conditions. This enhancement is primarily attributed to the increased specific surface area of the TiO₂/zeolite samples, making them promising materials for future efficient and sustainable photocatalytic applications.